乙基(2E)-2-氰基-3-(4-甲基苯基)丙烯酸酯合成路线 （共 12 条）
反应条件
1: 5 h / 180 °C 2: aq. NaOH / toluene / 2 h / 60 °C View Scheme
参考文献
Noda, Yumiki; Akiba, Yoshikazu; Kashima, Mikito
Synthetic Communications, 1996 , vol. 26, # 24 p. 4633 - 4639
反应条件
in acetonitrile T=20°C; Reduction; oxidation; 24 h; Kinetics; Further Variations:Temperatures;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 9 p. 1857 - 1861
反应条件
sodium hydroxide in methanol; water T=30°C; other temperatures; ΔH(excit.), ΔS(excit.); Rate constantThermodynamic dataKinetics;
参考文献
Journal of Chemical Research, Miniprint, , # 5 p. 980 - 997
反应条件
aluminum oxide in ethanol
0.583333 h; Heating;
参考文献
Mogilaiah; Babu, H. Sharath; Vidya; Kumar, K. Shiva
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2010 , vol. 49, # 3 p. 390 - 393
反应条件
recovered palladium catalyst in ethanol
T=20°C; 18 h; Green chemistry;
参考文献
Wang, Hu; Li, Li; Bai, Xing-Feng; Deng, Wen-Hui; Zheng, Zhan-Jiang; Yang, Ke-Fang; Xu, Li-Wen
Green Chemistry, 2013 , vol. 15, # 9 p. 2349 - 2355
反应条件
MS-SO3H(at)MS(at)MS-NH2 in toluene
T=80°C; 0.5 h; Reagent/catalyst;
参考文献
Li, Ping; Cao, Chang-Yan; Liu, Hua; Yu, Yu; Song, Wei-Guo
Journal of Materials Chemistry A, 2013 , vol. 1, # 41 p. 12804 - 12810
反应条件
sodium lauryl sulfate in water
T=25 - 30°C; 0.25 h;
参考文献
Sharma, Saikat Das; Gogoi, Pranjal; Konwar, Dilip
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2007 , vol. 46, # 10 p. 1672 - 1678
反应条件
1: 150 °C
2: hydrogen chloride
View Scheme
参考文献
Fiquet
Annales de Chimie (Cachan, France), 1893 , vol. <6> 29, p. 439
Bulletin de la Societe Chimique de France, 1901 , vol. <3> 25, p. 593
参考文献
Fiquet
Annales de Chimie (Cachan, France), 1893 , vol. <6> 29, p. 439
Bulletin de la Societe Chimique de France, 1901 , vol. <3> 25, p. 593
反应条件
1: 2-cyano-3-(p-tolyl)propionic acid ethyl ester With potassium hydride in acetonitrile
T=20°C; 0.333333 h; Inert atmosphereGlovebox;
2: 4-acetylamino-2,2,6,6-tetramethylpiperidine-1-oxoammonium in acetonitrile
T=24.84°C; Inert atmosphereGlovebox; Thermodynamic data;
参考文献
Cao, Ying; Zhang, Song-Chen; Zhang, Min; Shen, Guang-Bin; Zhu, Xiao-Qing
Journal of Organic Chemistry, 2013 , vol. 78, # 14 p. 7154 - 7168
