4-(三甲基甲硅烷基)吡啶合成路线 （共 15 条）
反应条件
1: With sodium methylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide 2 h; 2: With water Further stages.;
参考文献
Postigo; Rossi
Organic letters, 2001 , vol. 3, # 8 p. 1197 - 1200
反应条件
1: pyridine; hexamethyl-silane With sodium methylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide 0.25 h; 2: chloroformic acid ethyl ester Further stages.;
参考文献
Postigo; Rossi
Organic letters, 2001 , vol. 3, # 8 p. 1197 - 1200
反应条件
pyridine; lithium in tetrahydrofuran T=0°C; 1 h;
参考文献
Tsuge, Otohiko; Kanemasa, Shuji; Naritomi, Toshio; Tanaka, Junji
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 4 p. 1497 - 1504
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide 2 h;
参考文献
Postigo, Al; Vaillard, Santiago E.; Rossi, Roberto A.
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 12 p. 889 - 893
反应条件
iodine; magnesium in tetrahydrofuran T=70°C; 1 h;
参考文献
Effenberger, Franz; Krebs, Andreas; Willrett, Peter
Chemische Berichte, 1992 , vol. 125, # 5 p. 1131 - 1140
反应条件
n-butyllithium; potassium tert-butylate in tetrahydrofuran; hexane T=-105°C;
参考文献
Verbeek, Jacob; George, Albert V. E.; Jong, Robertus L. P. de; Brandsma, Lambert
Journal of the Chemical Society, Chemical Communications, 1984 , # 4 p. 257 - 258
反应条件
1: 34 percent / lithium, pyridine / tetrahydrofuran / 1 h / 0 °C 2: air View Scheme
参考文献
Tsuge, Otohiko; Kanemasa, Shuji; Naritomi, Toshio; Tanaka, Junji
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 4 p. 1497 - 1504
反应条件
1: lithium / tetrahydrofuran 2: air View Scheme
参考文献
Tsuge, Otohiko; Kanemasa, Shuji; Naritomi, Toshio; Tanaka, Junji
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 4 p. 1497 - 1504
反应条件
n-butyllithium; potassium tert-butylate THF / HMPT / hexane, 1) -100 deg C; Yield given. Multistep reaction;
参考文献
Barrett, Anthony G. M.; Dauzonne, Daniel; O'Neil, Ian A.; Renaud, Alain
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4409 - 4415
参考文献
Tsuge, Otohiko; Kanemasa, Shuji; Naritomi, Toshio; Tanaka, Junji
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 4 p. 1497 - 1504
