1-乙炔-4-((4-硝基苯基)乙炔)苯合成路线 （共 10 条）
反应条件
1: CuI, NEt3 / PdCl2(PPh3)2 2: K2CO3 / methanol 3: 66 percent / CuI, diethylamine / 4 h / Ambient temperature View Scheme
参考文献
Whittall, Ian R.; Cifuentes, Marie P.; Humphrey, Mark G.; Luther-Davies, Barry; Samoc, Marek; Houbrechts, Stephan; Persoons, Andre; Heath, Graham A.; Hockless, David C. R.
Journal of Organometallic Chemistry, 1997 , vol. 549, # 1-2 p. 127 - 137
反应条件
potassium tert-butylate in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Kondo, Koichi; Fujitani, Takumi; Ohnishi, Noriaki
Journal of Materials Chemistry, 1997 , vol. 7, # 3 p. 429 - 433
反应条件
copper(l) iodide; diethylamine 4 h; Ambient temperature;
参考文献
Whittall, Ian R.; Cifuentes, Marie P.; Humphrey, Mark G.; Luther-Davies, Barry; Samoc, Marek; Houbrechts, Stephan; Persoons, Andre; Heath, Graham A.; Hockless, David C. R.
Journal of Organometallic Chemistry, 1997 , vol. 549, # 1-2 p. 127 - 137
反应条件
1: K2CO3 / methanol 2: 66 percent / CuI, diethylamine / 4 h / Ambient temperature View Scheme
参考文献
Whittall, Ian R.; Cifuentes, Marie P.; Humphrey, Mark G.; Luther-Davies, Barry; Samoc, Marek; Houbrechts, Stephan; Persoons, Andre; Heath, Graham A.; Hockless, David C. R.
Journal of Organometallic Chemistry, 1997 , vol. 549, # 1-2 p. 127 - 137
反应条件
1: 22 percent / PdCl2(PPh3)2, CuI / diethylamine / 20 h / Ambient temperature 2: 78 percent / aq. NaOH / ethanol; tetrahydrofuran / 0.5 h View Scheme
参考文献
Lavastre, Olivier; Cabioch, Sandrine; Dixneuf, Pierre H.; Vohlidal, Jiri
Tetrahedron, 1997 , vol. 53, # 22 p. 7595 - 7604
反应条件
1: 22 percent / PdCl2(PPh3)2, CuI / diethylamine / 20 h / Ambient temperature 2: 78 percent / aq. NaOH / ethanol; tetrahydrofuran / 0.5 h View Scheme
参考文献
Lavastre, Olivier; Cabioch, Sandrine; Dixneuf, Pierre H.; Vohlidal, Jiri
Tetrahedron, 1997 , vol. 53, # 22 p. 7595 - 7604
反应条件
1: 65 percent / tetrahydrofuran / 3 h / Ambient temperature 2: 84 percent / POCl3, N,N-diethylaniline / 1 h / 90 °C 3: 44 percent / t-BuOK / tetrahydrofuran / 3 h / Ambient temperature View Scheme
参考文献
Kondo, Koichi; Fujitani, Takumi; Ohnishi, Noriaki
Journal of Materials Chemistry, 1997 , vol. 7, # 3 p. 429 - 433
反应条件
1: 84 percent / POCl3, N,N-diethylaniline / 1 h / 90 °C 2: 44 percent / t-BuOK / tetrahydrofuran / 3 h / Ambient temperature View Scheme
参考文献
Kondo, Koichi; Fujitani, Takumi; Ohnishi, Noriaki
Journal of Materials Chemistry, 1997 , vol. 7, # 3 p. 429 - 433
反应条件
NaOMe in methanol; dichloromethane N2-atmosphere; stirring (room temp., 16 h); evapn. (reduced pressure); elem. anal.;
参考文献
Whittall, Ian R.; Humphrey, Mark G.; Houbrechts, Stephan; Persoons, Andre; Hockless, David C. R.
Organometallics, 1996 , vol. 15, # 26 p. 5738 - 5745
反应条件
MeONa in methanol byproducts: NaCl; stirring of methanol soln. of Au chloride, alkyne and MeONa; identified by UV spectrum;
参考文献
Vicente, Jose; Teresa Chicote, Maria; Dolores Abrisqueta, Maria; Carmen Ramirez de Arellano; Jones, Peter G.; Humphrey, Mark G.; Cifuentes, Marie P.; Samoc, Marek; Luther-Davies, Barry
Organometallics, 2000 , vol. 19, # 16 p. 2968 - 2974
