triethylamine in tetrahydrofuran
byproducts: Et3N*HCl; dropwise addn. of Ge compd. soln. to soln. of MeP(O)(OH)2 and triethylamine with stirring; filtration; addn. of oxirane; stirring,2h; all under inert gas; detn. by NMR;
参考文献
Barrau, J.; Rima, G.; Satge, J.
Phosphorus, Sulfur, and Silicon and the Related Elements, 1990 , vol. 54, p. 23 - 30
triethylamine in 1,4-dioxane
T=24.9°C; enthalpy of reaction; Thermodynamic data;
参考文献
Ovchinnikov, V. V.; Brus'ko, V. V.; Cherkasov, R. A.
Russian Journal of General Chemistry, 1993 , vol. 63, # 3.2 p. 499 - 500
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 3 p. 707 - 708