5-乙基-1-甲基-4-硝基-1H-吡咯-2-羧酸合成路线 （共 6 条）
反应条件
sodium hydroxide in ethanol Heating;
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
反应条件
potassium hydroxide; oxygen in dimethyl sulfoxide 96 h; Ambient temperature;
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
反应条件
1: 81 percent / diethyl ether / 1 h 2: 68 percent / NaOEt / 0.5 h / Ambient temperature 3: 55 percent / 70percent HNO3 / 2 h / 30 °C 4: 77 percent / KOH / ethanol / 18 h / 0 °C 5: 70 percent / hexadecyl(tributyl)phosphonium bromide / acetonitrile / 24 h / Ambient temperature 6: 85 percent / 2 M aq. NaOH / ethanol / Heating View Scheme
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
反应条件
1: 55 percent / 70percent HNO3 / 2 h / 30 °C 2: 77 percent / KOH / ethanol / 18 h / 0 °C 3: 70 percent / hexadecyl(tributyl)phosphonium bromide / acetonitrile / 24 h / Ambient temperature 4: 85 percent / 2 M aq. NaOH / ethanol / Heating View Scheme
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
反应条件
1: 68 percent / NaOEt / 0.5 h / Ambient temperature 2: 55 percent / 70percent HNO3 / 2 h / 30 °C 3: 77 percent / KOH / ethanol / 18 h / 0 °C 4: 70 percent / hexadecyl(tributyl)phosphonium bromide / acetonitrile / 24 h / Ambient temperature 5: 85 percent / 2 M aq. NaOH / ethanol / Heating View Scheme
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
反应条件
1: 77 percent / KOH / ethanol / 18 h / 0 °C 2: 70 percent / hexadecyl(tributyl)phosphonium bromide / acetonitrile / 24 h / Ambient temperature 3: 85 percent / 2 M aq. NaOH / ethanol / Heating View Scheme
参考文献
Molins-Pujol, Antoni M.; Moranta, Concepcio; Arroyo, Carmina; Rodriguez, M. Teresa; Meca, M. Carmen; Pujol, M. Dolors; Bonal, Joaquim
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 18 p. 2277 - 2289
