1,3-二苄基四甲基二硅烷合成路线 （共 12 条）
反应条件
mercuric sulphate in sulfuric acid T=60 - 65°C; 2 h;
参考文献
Karaev, S. F.; Kuliev, R. M.; Guseinov, Sh. O.; Askerov, M. E.; Movsumzade, M. M.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 5 p. 1160 - 1163,1016 - 1019
反应条件
sodium hydroxide in diethyl ether T=0°C; 0.333333 h;
参考文献
Wrobel, Dieter; Tacke, Reinhold; Wannagat, Ulrich; Harder, Ulrich
Chemische Berichte, 1982 , vol. 115, # 5 p. 1694 - 1704
反应条件
water in diethyl ether 1 h;
参考文献
Kabachnik, M. I.; Zakharov, L. S.; Molchanova, G. N.; Drozdova, T. D.; Petrovskii, P. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 7.2 p. 1527 - 1532
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , vol. 38, # 7 p. 1664 - 1670
反应条件
potassium hydroxide in ethanol; water 18 h; Ambient temperature;
参考文献
Wrobel, Dieter; Wannagat, Ulrich; Harder, Ulrich
Monatshefte fuer Chemie, 1982 , vol. 113, p. 381 - 388
反应条件
hydrogenchloride in methanol; water
参考文献
Eaborn, Colin; Stanczyk, Wlodzimierz
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 2099 - 2104
参考文献
Mitsudome, Takato; Noujima, Akifumi; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
Chemical Communications, 2009 , # 35 p. 5302 - 5304
反应条件
1: 40 percent / tetrahydrofuran / 6 h / Heating 2: 40 percent / HgSO4 / H2SO4 / 2 h / 60 - 65 °C View Scheme
参考文献
Wrobel, Dieter; Wannagat, Ulrich; Harder, Ulrich
Monatshefte fuer Chemie, 1982 , vol. 113, p. 381 - 388
反应条件
1: 58 percent / CHCl3 2: 38 percent / KOH / H2O; ethanol / 18 h / Ambient temperature View Scheme
参考文献
Wrobel, Dieter; Wannagat, Ulrich; Harder, Ulrich
Monatshefte fuer Chemie, 1982 , vol. 113, p. 381 - 388
反应条件
potassium acetate T=240 - 250°C;
参考文献
Pola,J. et al.
Collection of Czechoslovak Chemical Communications, 1973 , vol. 38, p. 1522 - 1527
反应条件
1: 1) Mg, iodine / 1) Et2O, 1 h, reflux, 2) Et2O 2: 50 percent / NaOH / diethyl ether / 0.33 h / 0 °C View Scheme
参考文献
Wrobel, Dieter; Tacke, Reinhold; Wannagat, Ulrich; Harder, Ulrich
Chemische Berichte, 1982 , vol. 115, # 5 p. 1694 - 1704
