2-(三甲基硅氧基)丙烯合成路线 (共 98 条)
反应条件
boron trifluoride diethyl etherate in tetrahydrofuran T=-78 - 0°C;
参考文献
Sasaki, Mikio; Yudin, Andrei K.
Synlett, 2004 , # 13 p. 2443 - 2444
反应条件
T=40°C; 40 h; Irradiation; Further byproducts given;
参考文献
Voronkov, M. G.; Rakhlin, V. I.; Khangazeev, S. Kh.; Mirskov, R. G.; Dneprovskii, A. S.
Doklady Chemistry, 1981 , vol. 259, p. 386 - 388
Dokl. Akad. Nauk SSSR Ser. Khim., 1981 , vol. 259, # 6 p. 1364 - 1366
反应条件
triethyl borane in hexane; dimethyl sulfoxide Ambient temperature;
参考文献
Baciocchi, Enrico; Muraglia, Ester
Tetrahedron Letters, 1994 , vol. 35, # 17 p. 2763 - 2766
反应条件
BnNMe3(+)F(-) in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Hirsch, Elisabeth; Huenig, Siegfried; Reissig, Hans-Ulrich
Chemische Berichte, 1982 , vol. 115, # 12 p. 3687 - 3696
反应条件
cycloocta-1,5-diene{1,4-bis(diphenylphosphino)butane}rhodium perchlorate in dichloromethane T=100°C; 16 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 352, p. 223 - 238
反应条件
Nafion-TMS in dichloromethane T=-78 - 20°C; 18 h; Yield given;
参考文献
Haunert, Frank; Bolli, Martin H.; Hinzen, Berthold; Ley, Steven V.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 15 p. 2235 - 2237
反应条件
manganese(II) fluoride; ZnF2; tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=70°C;
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 35 p. 5852 - 5855
反应条件
sodium hydroxide; formic acid; water; sodium chloride in acetonitrile T=25°C; Rate constantMechanism;
参考文献
Novice, Marilyn H.; Seikaly, Hani R.; Seiz, Annette D.; Tidwell, Thomas T.
Journal of the American Chemical Society, 1980 , vol. 102, # 18 p. 5835 - 5838
反应条件
(difluoroiodo)benzene-boron trifluoride in dichloromethane T=-78 - 20°C;
参考文献
Zefirov, N. S.; Samoniya, N. Sh.; Kutateladze, T. G.; Zhdankin, V. V.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 1.2 p. 194 - 195
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 1 p. 220 - 222
反应条件
manganese(II) fluoride; ZnF2; tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=70°C;
参考文献
Su, Weiping; Raders, Steven; Verkade, John G.; Liao, Xuebin; Hartwig, John F.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 35 p. 5852 - 5855