2-(三甲基硅氧基)丙烯合成路线 （共 98 条）
反应条件
tetrabutyl ammonium fluoride; fluorine 1.) CH2Cl2, not above -50 deg C, 2.) CH2Cl2, a) -50 deg C, 1 h, b) -50 to 0 deg C, 1 h, c) 0 deg C, 0.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kiselyov, Alexander S.; Strekowski, Lucjan
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4476 - 4478
反应条件
(i) TiCl4, CH2Cl2, (ii) TsOH, benzene; Multistep reaction;
参考文献
Banno,K.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 2284 - 2291
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-78°C;
参考文献
Turcaud, Serge; Martens, Thierry; Sierecki, Emma; Perard-Viret, Joelle; Royer, Jacques
Tetrahedron Letters, 2005 , vol. 46, # 31 p. 5131 - 5134
反应条件
tetrabutyl ammonium fluoride; fluorine 1.) CH2Cl2, not above -50 deg C, 2.) CH2Cl2, a) -50 deg C, 1 h, b) -50 to 0 deg C, 1 h, c) 0 deg C, 0.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kiselyov, Alexander S.; Strekowski, Lucjan
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4476 - 4478
反应条件
in benzene T=10 - 15°C; 4 h; Irradiation;
参考文献
Shimizu, Nobujiro; Yamaoka, Shintaro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3853 - 3854
反应条件
Ambient temperature;
参考文献
Antonsen, Oeyvind; Benneche, Tore; Gundersen, Lise-Lotte; Undheim, Kjell
Acta Chemica Scandinavica, 1992 , vol. 46, # 2 p. 172 - 177
反应条件
in acetonitrile 1 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 62, # 9 p. 2742 - 2751
反应条件
[Rh(I)(cycloocta-1,5-diene)(butane-1,4-diylbis[diphenylphosphine])]ClO4 in dichloromethane
T=100°C; 15 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 352, p. 223 - 238
反应条件
tris(pentafluorophenyl)-borane; hydrogen; dppn in benzene
T=20°C; P=45004.5 Torr; 3 h;
参考文献
Wang, Huadong; Froehlich, Roland; Kehr, Gerald; Erker, Gerhard
Chemical Communications, 2008 , # 45 p. 5966 - 5968
反应条件
zinc(II) chloride in dichloromethane
T=-25°C; 4 h;
参考文献
Reetz, Manfred T.; Mueller-Starke, H.
Liebigs Annalen der Chemie, 1983 , # 10 p. 1726 - 1738
