2-(三甲基硅氧基)丙烯合成路线 （共 98 条）
反应条件
zinc(II) iodide in diethyl ether
T=22°C; 2 h;
参考文献
Reetz, Manfred T.; Mueller-Starke, H.
Liebigs Annalen der Chemie, 1983 , # 10 p. 1726 - 1738
反应条件
in acetonitrile
1 h; Irradiation;
参考文献
Moran, Ricardo J.; Cramer, Christopher; Falvey, Daniel E.
Journal of Organic Chemistry, 1997 , vol. 62, # 9 p. 2742 - 2751
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris(dibenzylideneacetone)dipalladium (0); ZnF2 in N,N-dimethyl-formamide
T=150°C; 0.25 h; Irradiationmicrowave;
参考文献
Chobanian, Harry R.; Liu, Ping; Chioda, Marc D.; Guo, Yan; Lin, Linus S.
Tetrahedron Letters, 2007 , vol. 48, # 7 p. 1213 - 1216
反应条件
1: With bismuth trifluoromethanesulphonate in acetonitrile
T=25°C;
2: With silica gel in hexane; ethyl acetate
参考文献
Ollevier, Thierry; Nadeau, Etienne
Journal of Organic Chemistry, 2004 , vol. 69, # 26 p. 9292 - 9295
反应条件
zinc tetrafluoroborate in tetrahydrofuran; water
T=28 - 30°C; Mannich reaction; 0.166667 h;
参考文献
x
Tetrahedron, 2002 , vol. 58, # 5 p. 983 - 988
反应条件
potassium tert-butylate
1) THF, -30 deg C, 40 min; 2) THF, -30 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Duhamel, Pierre; Cahard, Dominique; Poirier, Jean-Marie
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 21 p. 2509 - 2512
反应条件
dodecacarbonyltetrarhodium(0) in benzene
T=100°C; 16 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Tetrahedron Letters, 1986 , vol. 27, # 45 p. 5517 - 5520
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Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 352, p. 223 - 238
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate; bismuth trifluoromethanesulphonate
T=25°C; Mukaiyama aldol reaction; 22 h;
参考文献
Ollevier, Thierry; Desyroy, Valerie; Debailleul, Blandine; Vaur, Sophie
European Journal of Organic Chemistry, 2005 , # 23 p. 4971 - 4973
反应条件
1: 1-pyrrolidincarbonsaure-methylester With trifluorormethanesulfonic acid; tetra-n-butylammonium tetrafluoroborate in dichloromethane
T=-72°C; Electrochemical reaction;
2: isopropenyloxy trimethylsilane in dichloromethane
T=-28°C; Further stages.;
参考文献
Suga; Okajima; Fujiwara; Yoshida
Journal of the American Chemical Society, 2001 , vol. 123, # 32 p. 7941 - 7942
反应条件
N-chloro-succinimide in dichloromethane
Heating;
参考文献
Hambly, G. F.; Chan, T. H.
Tetrahedron Letters, 1986 , vol. 27, # 23 p. 2563 - 2566
