2-(三甲基硅氧基)丙烯合成路线 （共 98 条）
反应条件
piperidin-2-one in 1-methyl-pyrrolidin-2-one
T=20°C;
参考文献
Suginome, Michinori; Uehlin, Lars; Murakami, Masahiro
Journal of the American Chemical Society, 2004 , vol. 126, # 41 p. 13196 - 13197
反应条件
[Rh(1,5-cyclooctadiene)(PMePh2)2]OTf in dichloromethane
T=80°C; Substitution; 19 h; Title compound not separated from byproducts;
参考文献
Muraoka; Matsuda; Itoh
Tetrahedron Letters, 2000 , vol. 41, # 45 p. 8807 - 8811
反应条件
[Rh(1,5-cyclooctadiene)(PMePh2)2]OTf in acetonitrile
T=80°C; Substitution; 19 h; Title compound not separated from byproducts;
参考文献
Muraoka; Matsuda; Itoh
Tetrahedron Letters, 2000 , vol. 41, # 45 p. 8807 - 8811
反应条件
[Ir(cod)(PPh3)2]OTf; hydrogen in dichloromethane
T=25°C; 1 h; Title compound not separated from byproducts;
参考文献
Matsuda, Isamu; Wakamatsu, Shogo; Komori, Ken-Ichi; Makino, Tatsuya; Itoh, Kenji
Tetrahedron Letters, 2002 , vol. 43, # 6 p. 1043 - 1046
反应条件
in dichloromethane
T=0°C; 4 h;
参考文献
Akiba, Kin-ya; Nishihara, Yoshihiro; Wada, Makoto
Tetrahedron Letters, 1983 , vol. 24, # 47 p. 5269 - 5272
反应条件
1.) CH2Cl2, 2.) CH2Cl2; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Akiba, Kin-ya; Nishihara, Yoshihiro; Wada, Makoto
Heterocycles, 1984 , vol. 21, # 2 p. 536
反应条件
in dichloromethane
T=0°C; 4 h;
参考文献
Akiba, Kin-ya; Nishihara, Yoshihiro; Wada, Makoto
Tetrahedron Letters, 1983 , vol. 24, # 47 p. 5269 - 5272
反应条件
1.) CH2Cl2, 2.) CH2Cl2; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Akiba, Kin-ya; Nishihara, Yoshihiro; Wada, Makoto
Heterocycles, 1984 , vol. 21, # 2 p. 536
反应条件
in benzene
T=10 - 15°C; 4 h; Irradiation;
参考文献
Shimizu, Nobujiro; Yamaoka, Shintaro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3853 - 3854
反应条件
in benzene
T=10 - 15°C; 4 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Shimizu, Nobujiro; Yamaoka, Shintaro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3853 - 3854
