4,4,5,5-四氟-1,3-二氧戊环-2-酮合成路线 (共 3 条)
反应条件
fluorine T=35.3 - 36.4°C; P=4372.94 Torr; Inert atmosphere;
参考文献
SOLVAY FLUOR GmbH; OLSCHIMKE, Jens; SEFFER, Dirk; BOMKAMP, Martin
Patent: WO2011/36283 A2, 2011 ;
Location in patent: Page/Page column 11-13 ;
反应条件
hydrogen fluoride T=-40°C; Electrochemical reactionnickel electrodes;
参考文献
SOLVAY FLUOR GmbH; BOMKAMP, Martin; OLSCHIMKE, Jens; EICHER, Johannes
Patent: WO2011/48053 A1, 2011 ;
Location in patent: Page/Page column 11-12 ;
反应条件
1: With chlorine T=40 - 120°C; Photochemical reactorUV light lamp-irradiationInert atmosphere; 2: With triethylamine tris(hydrogen fluoride); triethylamine T=80 - 100°C; Product distribution / selectivity;
参考文献
SOLVAY FLUOR GmbH; BOMKAMP, Martin; OLSCHIMKE, Jens; EICHER, Johannes
Patent: WO2011/48053 A1, 2011 ;
Location in patent: Page/Page column 10 ;