4-甲酰基哌嗪-1-羧酸叔丁酯合成路线 （共 7 条）
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O; water; oxygen; silica gel; caesium carbonate in acetonitrile T=20°C; 60 h; Inert atmosphereIrradiation;
参考文献
Zhao, Yaohong; Cai, Shunyou; Li, Jing; Wang, David Zhigang
Tetrahedron, 2013 , vol. 69, # 38 p. 8129 - 8131
反应条件
in tetrahydrofuran T=20°C; 2 h;
参考文献
Murai, Toshiaki; Asai, Fumio
Journal of the American Chemical Society, 2007 , vol. 129, # 4 p. 780 - 781
反应条件
sodium ethanolate T=50°C; Riemer-Tiemann reaction; Inert atmosphere;
参考文献
Shastri, Lokesh A.; Shastri, Samundeeswari L.; Bathula, Chinna D.; Basanagouda, Mahantesha; Kulkarni, Manohar V.
Synthetic Communications, 2011 , vol. 41, # 4 p. 476 - 484
反应条件
oxalyl dichloride; triethylamine in dichloromethane; dimethyl sulfoxide T=-78 - 2°C; Swern oxidation;
参考文献
Ishikawa, Makoto; Furuuchi, Takeshi; Yamauchi, Miki; Yokoyama, Fumikazu; Kakui, Nobukazu; Sato, Yasuo
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 14 p. 5441 - 5448
反应条件
1: 4-(N,N-dimethlyamino)pyridine / dichloromethane 2: hydrogenchloride / acetonitrile; water / 25 °C View Scheme
参考文献
Kang, Ji-Sun; Lee, Jae-In; Um, Ik-Hwan
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 9 p. 2971 - 2975
反应条件
1: potassium carbonate / toluene / 6 h / |Reflux; |Inert atmosphere 2: [Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O; oxygen; silica gel; water; caesium carbonate / acetonitrile / 60 h / 20 °C / |Inert atmosphere; |Irradiation View Scheme
参考文献
Zhao, Yaohong; Cai, Shunyou; Li, Jing; Wang, David Zhigang
Tetrahedron, 2013 , vol. 69, # 38 p. 8129 - 8131
反应条件
hydrogenchloride in water; acetonitrile T=25°C; Kinetics;
参考文献
Kang, Ji-Sun; Lee, Jae-In; Um, Ik-Hwan
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 9 p. 2971 - 2975
