反应条件
1: 100 percent / TMSCl / 12 h / Ambient temperature
2: 89 percent / methanol / 20 h / Heating
3: 1.) n-BuLi / 1.) heptane, hexane, 0 deg C, 30 min, 2.) hexane, heptane, -30 deg C - 0 deg C, 1 h
4: 71 percent / NaBH4, n-Bu4NCl / H2O / 18 h
View Scheme
参考文献
Henegar; Ashford; Baughman; Sih; Gu
Journal of Organic Chemistry, 1997 , vol. 62, # 19 p. 6588 - 6597
