反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '110700', constants.ctx, '0')">thiazoline-2,4-dione</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '4122952', constants.ctx, '0')">sodium hydride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '8190416', constants.ctx, '0')">mineral oil</a> <br />T=20°C; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '506256', constants.ctx, '0')">2-bromo-acetic acid methyl ester</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a>; <a href="#" onclick="return RXDsubstances(event, this, '8190416', constants.ctx, '0')">mineral oil</a> <br />3 h; Cooling with iceReflux; <br />
参考文献
Nishida, Sho; Maruoka, Hiroshi; Yoshimura, Yuki; Goto, Takao; Tomita, Ryoko; Masumoto, Eiichi; Okabe, Fumi; Yamagata, Kenji; Fujioka, Toshihiro Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 2 p. 303 - 309
