4-(苄氧基)-3-甲氧基苯甲酰甲基溴化物合成路线 （共 13 条）
反应条件
copper(ll) bromide in ethanol; chloroform T=70°C; 0.25 h; Microwave irradiation;
参考文献
Ouyang, Xin-Ping; Liu, Chun-Lei; Pang, Yu-Xia; Qiu, Xue-Qing
Chinese Chemical Letters, 2013 , vol. 24, # 12 p. 1091 - 1094
反应条件
bromine in chloroform
参考文献
Fuglseth, Erik; Anthonsen, Thorleif; Hoff, Bard Helge
Tetrahedron Asymmetry, 2006 , vol. 17, # 8 p. 1290 - 1295
反应条件
1: 97 percent / K2CO3 / dimethylformamide / 1 h / 100 °C 2: 38 percent / Br2 / CHCl3 View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 17, # 8 p. 1290 - 1295
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 80 °C / |Microwave irradiation 2: copper(ll) bromide / ethanol; chloroform / 0.25 h / 70 °C / |Microwave irradiation View Scheme
参考文献
Chinese Chemical Letters, , vol. 24, # 12 p. 1091 - 1094
反应条件
1: 97 percent / K2CO3 / dimethylformamide / 1 h / 100 °C 2: 38 percent / Br2 / CHCl3 View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 17, # 8 p. 1290 - 1295
反应条件
1: 95 percent / K2CO3 / dimethylformamide / 2 h / 25 °C 2: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h 3: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C 4: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation View Scheme
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 83 percent 2: 91 percent 3: 1.) NaBH4; 2.) H2 / 1.) dioxane; 2.) ethanol View Scheme
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 95 percent / K2CO3 / dimethylformamide / 2 h / 25 °C 2: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h 3: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C 4: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation 5: 99 percent / pyridine / 0.17 h / 5 °C View Scheme
参考文献
Tetrahedron, , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 95 percent / K2CO3 / dimethylformamide / 2 h / 25 °C
2: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h
3: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C
4: 28 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation
View Scheme
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 95 percent / K2CO3 / dimethylformamide / 2 h / 25 °C
2: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h
View Scheme
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
