1-氯-2,3,5,6-四氟苯合成路线 （共 8 条）
反应条件
chlorine T=400°C; 0.305 h;
参考文献
Platonov; Maksimov; Dvornikova; Nikul'shin
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 11 p. 1647 - 1653
反应条件
monomethyldichlorosilane T=140 - 170°C; (electron irradiation);
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 47, # 4 p. 782 - 785,713 - 716
反应条件
t-Bu-XantPhos; tBuXantphosAu(AuCl2); (Ph)2SiH2; acetic acid in 1,2-dichloro-ethane T=80°C; 24 h; Inert atmosphere;
参考文献
Zhan, Jin-Hui; Lv, Hongbin; Yu, Yi; Zhang, Jun-Long
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1529 - 1541
反应条件
sodium dithionite in N,N-dimethyl-formamide T=110 - 115°C; 54 h; Yield given. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 50, # 2 p. 151 - 172
反应条件
1: KSH / dimethylformamide / 45 - 55 °C 2: 93 percent / Cl2 / 0.3 h / 400 °C View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 41, # 11 p. 1647 - 1653
参考文献
Journal of the Chemical Society, , p. 3372 - 3379
反应条件
hydroxymethanesulfinic acid sodium salt; sodium hydrogencarbonate in N,N-dimethyl-formamide 43 to 113 deg C, 57h to 1 week; Yield given. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 50, # 2 p. 151 - 172
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 38, # 3 p. 519 - 524,510 - 514
