1,3-双(4-氯苯基)-1,3-丙二酮合成路线 （共 17 条）
反应条件
sodium ethanolate
T=160 - 180°C;
参考文献
McElvain; Weber
Journal of the American Chemical Society, 1941 , vol. 63, p. 2192,2193
反应条件
2,2,6,6-tetramethyl-piperidine; n-butyllithium in tetrahydrofuran; hexane
参考文献
Reitz,D.B. et al.
Journal of the American Chemical Society, 1978 , vol. 100, p. 5428 - 5436
反应条件
[2,2']bipyridinyl; palladium (II) trifluoroacetate; water; trifluoroacetic acid in tetrahydrofuran
T=80°C; 36 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Xingyong; Liu, Miaochang; Xu, Long; Wang, Qingzong; Chen, Jiuxi; Ding, Jinchang; Wu, Huayue
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5273 - 5281
反应条件
sodium hydride in benzene
3 h;
参考文献
Choshi; horimoto; Wang; Nagase; Ichikawa; Sugino; Hibino
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 4 p. 1047 - 1049
反应条件
1: 87 percent / conc. H2SO4 / 3 h / Heating
2: 55 percent / NaH / benzene / 3 h
View Scheme
参考文献
Choshi; horimoto; Wang; Nagase; Ichikawa; Sugino; Hibino
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 4 p. 1047 - 1049
参考文献
Sieglitz; Horn
Chemische Berichte, 1951 , vol. 84, p. 607,615
反应条件
(i) AlCl3, (ii) aq. HCl; Multistep reaction;
参考文献
Dayer,F. et al.
Helvetica Chimica Acta, 1974 , vol. 57, # 7 p. 2201 - 2209
