1,3-双(4-甲氧基苯基)1,3-丙二酮合成路线 (共 26 条)
反应条件
1,3-dibenzyl-1H-benzo[d]imidazol-3-ium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=20°C; 0.366667 h; Inert atmosphere;
参考文献
Singh, Santosh; Singh, Pankaj; Rai, Vijai K.; Kapoor, Ritu; Yadav, Lal Dhar S.
Tetrahedron Letters, 2011 , vol. 52, # 1 p. 125 - 128
反应条件
1: 1-(4-methoxyphenyl)ethanone With lithium hexamethyldisilazane in toluene T=0°C; 2: methyl 4-(N-tert-butoxycarbonyl-(5S)-methyl-(2S)-pyrrolidinylmethoxy)benzoate in toluene Further stages.;
参考文献
Dhondi, Pawan K.; Carberry, Patrick; Chisholm, John D.
Tetrahedron Letters, 2007 , vol. 48, # 49 p. 8743 - 8746
反应条件
1: 4-methoxy-benzoyl chloride With aluminium trichloride in various solvent(s) T=55°C; 2 h; 2: vinyl acetate in various solvent(s) T=55°C; 20 h; Further stages.;
参考文献
Cogne-Laage, Emmanuelle; Allemand, Jean-Francois; Ruel, Odile; Baudin, Jean-Bernard; Croquette, Vincent; Blanchard-Desce, Mireille; Jullien, Ludovic
Chemistry - A European Journal, 2004 , vol. 10, # 6 p. 1445 - 1455
反应条件
anhydrous iron chloride in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Nomura, Kenichi; Asano, Keisuke; Kurahashi, Takuya; Matsubara, Seijiro
Heterocycles, 2008 , vol. 76, # 2 p. 1381 - 1399
参考文献
Ohta, Kazuchika; Muroki, Hiromitsu; Hatada, Koh-Ichi; Takagi, Akira; Ema, Hiroshi; et al.
Molecular Crystals and Liquid Crystals (1969-1991), 1986 , vol. 140, p. 163 - 178
反应条件
samarium (III) iodide in acetonitrile T=70°C; 3 h;
参考文献
Hao, Wenying; Zhang, Yongmin; Ying, Taokai; Lu, Pin
Synthetic Communications, 1996 , vol. 26, # 12 p. 2421 - 2427
反应条件
2,2,6,6-tetramethyl-piperidine; n-butyllithium in tetrahydrofuran; hexane
参考文献
Journal of the American Chemical Society, , vol. 100, p. 5428 - 5436
反应条件
sodium hydride in cyclohexane 2 h; Heating;
参考文献
Yamada, Tohru; Takai, Toshihiro; Rhode, Oliver; Mukaiyama, Teruaki
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 7 p. 2109 - 2117
反应条件
lithium hexamethyldisilazane Claisen condensation;
参考文献
Vijaykumar, Dange; Katzenellenbogen, John A.
Journal of Labelled Compounds and Radiopharmaceuticals, 2001 , vol. 44, p. S342 - S344