N,4-二甲基-苯甲酰胺合成路线 （共 34 条）
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane
T=160°C; 0.333333 h; Microwave irradiation;
参考文献
Odell, Luke R.; Saevmarker, Jonas; Larhed, Mats
Tetrahedron Letters, 2008 , vol. 49, # 42 p. 6115 - 6118
反应条件
dicobalt octacarbonyl in benzene
T=180°C; P=56886.3 - 67229.2 Torr; stainless steel autoclave; Further byproducts given;
参考文献
Antebi, Shlomo; Alper, Howard
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2010 - 2012
反应条件
dicobalt octacarbonyl in benzene
T=180°C; P=56886.3 - 67229.2 Torr; stainless steel autoclave; Further byproducts given;
参考文献
Antebi, Shlomo; Alper, Howard
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2010 - 2012
反应条件
dicobalt octacarbonyl in benzene
T=180°C; P=56886.3 - 67229.2 Torr; stainless steel autoclave; Further byproducts given;
参考文献
Antebi, Shlomo; Alper, Howard
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2010 - 2012
反应条件
silica gel; caesium carbonate; 1-(toluene-p-sulphonyl)imidazole in N,N-dimethyl-formamide
Beckmann rearrangement; 1.5 h; Reflux;
参考文献
Rad, Mohammad Navid Soltani; Khalafi-Nezhad, Ali; Behrouz, Somayeh; Amini, Zohreh; Behrouz, Marzieh
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 8 p. 1658 - 1671
反应条件
water; oxygen in gas
T=46.9°C; P=750.06 Torr; Irradiationcompetition reaction with PhCN, var. pressure; k/k0; other substrates; Product distribution;
参考文献
Attina, Marina; Cacace, Fulvio; Ricci, Andreina
Angewandte Chemie, 1991 , vol. 103, # 11 p. 1527 - 1529
反应条件
pyridine in chloroform-d1
T=25°C;
参考文献
Banks, Malcom R.; Hudson, Robert F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 463 - 468
反应条件
pyridine in chloroform-d1
T=25°C;
参考文献
Banks, Malcom R.; Hudson, Robert F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 463 - 468
反应条件
1.1: lithium chloride; magnesium / tetrahydrofuran / 2 h / 20 °C / |Inert atmosphere
1.2: 0.5 h / 0 °C / |Inert atmosphere
1.3: 2 h / 20 °C / |Inert atmosphere
2.1: tetrahydrofuran; water / 1 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
European Journal of Organic Chemistry, 2013 , # 34 p. 7815 - 7822
反应条件
pyridine in chloroform-d1
T=25°C;
参考文献
Banks, Malcom R.; Hudson, Robert F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 463 - 468
