N,4-二甲基-苯甲酰胺合成路线 （共 34 条）
反应条件
1: PCl5
2: KOH-solution
View Scheme
参考文献
van Scherpenzeel
Recueil des Travaux Chimiques des Pays-Bas, 1901 , vol. 20, p. 155
反应条件
in tetrahydrofuran; water
T=20°C; 1 h; Inert atmosphere;
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
European Journal of Organic Chemistry, 2013 , # 34 p. 7815 - 7822
反应条件
1: sodium carbonate
2: pyridine / CDCl3 / 25 °C
View Scheme
参考文献
Banks, Malcom R.; Hudson, Robert F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 463 - 468
反应条件
in acetonitrile
T=40°C; 0.5 h; Inert atmosphereUV-irradiation; TemperatureReagent/catalystConcentrationTime;
参考文献
Zhang, Yuan; Blackman, Melissa L.; Leduc, Andrew B.; Jamison, Timothy F.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 15 p. 4251 - 4255
Angew. Chem., 2013 , vol. 125, # 15 p. 4345 - 4349,5
反应条件
in chloroform-d1
6 h; Ambient temperature;
参考文献
Hoffman, Robert V.; Salvador, James M.
Journal of Organic Chemistry, 1992 , vol. 57, # 16 p. 4487 - 4490
参考文献
Ankers,W.B. et al.
Journal of the Chemical Society, Chemical Communications, 1972 , p. 935 - 936
反应条件
aluminium trichloride
参考文献
Gattermann; Schmidt
Justus Liebigs Annalen der Chemie, 1888 , vol. 244, p. 52
Chemische Berichte, 1887 , vol. 20, p. 860
反应条件
1: 81 percent / CH2Cl2 / 73 h / Ambient temperature
2: 0.5 h / 180 - 185 °C
View Scheme
参考文献
Friedrichsen, Willy; Kujath, Eckard; Liebezeit, Gerd
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1982 , vol. 37, # 2 p. 222 - 233
反应条件
1: Reaktion ueber mehrere Stufen
2: concentrated sulfuric acid; H2O
3: PCl5
4: KOH-solution
View Scheme
参考文献
van Scherpenzeel
Recueil des Travaux Chimiques des Pays-Bas, 1901 , vol. 20, p. 155
反应条件
1: concentrated sulfuric acid; H2O
2: PCl5
3: KOH-solution
View Scheme
参考文献
van Scherpenzeel
Recueil des Travaux Chimiques des Pays-Bas, 1901 , vol. 20, p. 155
