反应条件
1: 39 percent / bis(dibenzylidenacetone)palladium, Ph3P, 1,2-bis(diphenylphosphine)ethane, AcOH / 20 h / Ambient temperature 2: NaH / 1.) THF, reflux, 1 h, 2.) room temperature 3: <Rh((RS)-(6,6'-dimethylbiphenyl-2,2'-diyl)-bis(diphenylphosphine))((Z,Z)-1,5-cycloctadiene)>BF4 / tetrahydrofuran / 38 h / 90 °C 4: 96 percent / Ag2O View Scheme
参考文献
Schmid, Rudolf; Hansen, Hans-Juergen
Helvetica Chimica Acta, 1990 , vol. 73, p. 1258 - 1275