2-(氯甲基)烯丙基-三甲基硅烷合成路线 (共 11 条)
反应条件
lithium chloride in tetrahydrofuran T=40°C; 18 h;
参考文献
Clive, Derrick L. J.; Paul, Christine Chua; Wang, Zhongren
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 7028 - 7032
反应条件
pyridine; thionyl chloride in dichloromethane 0.5 h; Ambient temperature;
参考文献
Jones, Michael D.; Kemmitt, Raymond D. W.; Platt, Andrew W. G.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1986 , p. 1411 - 1418
反应条件
in diethyl ether 1.) -78 deg C, 1 h, 2.) RT, 10 h;
参考文献
Trost, Barry M.; Buch, Michael; Miller, Maria L.
Journal of Organic Chemistry, 1988 , vol. 53, # 20 p. 4887 - 4888
反应条件
cerium(III) chloride
参考文献
Lee, Thomas V.; Porter, John R.; Roden, Frances S.
Tetrahedron Letters, 1988 , vol. 29, # 39 p. 5009 - 5012
参考文献
Tetrahedron Letters, , vol. 21, # 47 p. 4557 - 4560
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , # 3 p. 428 - 435
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 461 - 468
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 243,245, 247; engl. Ausg. S. 233, 235, 236
反应条件
in N,N-dimethyl-formamide T=55 - 60°C; 48 h;
参考文献
Trost, Barry M.; Buch, Michael; Miller, Maria L.
Journal of Organic Chemistry, 1988 , vol. 53, # 20 p. 4887 - 4888
反应条件
in tetrahydrofuran T=35 - 45°C; 2 h; Irradiation; Product distribution; Further Variations:Solvents;
参考文献
Journal of the Chinese Chemical Society, , vol. 48, # 6 B p. 1129 - 1134
反应条件
sodium hydride 1.) DMF, 20 deg C, 2.) DMF, 20 deg C; Yield given. Multistep reaction;
参考文献
Krief, Alain; Dumont, Willy; Marko, Istvan E.; Murphy, Fiona; Vanherck, Jean-Christophe; Duval, Romain; Ollevier, Thierry; Abel, Ulrich
Synlett, 1998 , # 11 p. 1219 - 1222
参考文献
Knapp, Spencer; O'Connor, Una; Mobilio, Dominick
Tetrahedron Letters, 1980 , vol. 21, # 47 p. 4557 - 4560