2-苯基-1-苯并呋喃合成路线 (共 220 条)
反应条件
1: sodium; ethanol 2: K2CO3; acetone View Scheme
参考文献
Journal of the Chemical Society, , p. 3544,3545
反应条件
potassium carbonate in ethanol
T=80°C; Suzuki coupling; 12 h; Inert atmosphere;
参考文献
Hoshiya, Naoyuki; Shuto, Satoshi; Arisawa, Mitsuhiro
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 743 - 748
反应条件
bis(η3-allyl-μ-chloropalladium(II)); N,N,N′,N′-tetra(diphenylphosphinomethyl)pyridine-2,6-diamine; caesium carbonate in N,N-dimethyl-formamide
T=130°C; Sonogashira Cross-Coupling; 1 h; Schlenk techniqueInert atmosphere;
参考文献
Zhou, Rong; Wang, Wei; Jiang, Zhi-Jie; Wang, Kun; Zheng, Xue-Li; Fu, Hai-Yan; Chen, Hua; Li, Rui-Xiang
Chemical Communications, 2014 , vol. 50, # 45 p. 6023 - 6026
反应条件
potassium phosphate; palladium bis(2,2,6,6-tetramethyl-3,5-heptanedionate) in 1-methyl-pyrrolidin-2-one
T=140°C; 48 h;
参考文献
Nandurkar, Nitin S.; Bhanushali, Mayur J.; Bhor, Malhari D.; Bhanage, Bhalchandra M.
Tetrahedron Letters, 2008 , vol. 49, # 6 p. 1045 - 1048
反应条件
oxygen; acetic acid; palladium diacetate
T=120°C; P=2280.15 Torr; 1.5 h;
参考文献
Dwight, Timothy A.; Rue, Nicholas R.; Charyk, Dagmara; Josselyn, Ryan; DeBoef, Brenton
Organic Letters, 2007 , vol. 9, # 16 p. 3137 - 3139
反应条件
sodium tert-pentoxide in toluene
Heating;
参考文献
Hercouet, A.; Corre, M. Le
Tetrahedron, 1981 , vol. 37, # 16 p. 2867 - 2874
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in 1-methyl-pyrrolidin-2-one
T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L.N.; Awasthi, Dheeraj K.; Talode, Jalindar B.
Tetrahedron Letters, 2012 , vol. 53, # 21 p. 2662 - 2666
反应条件
[2,2']bipyridinyl; palladium diacetate; trifluoroacetic acid in tetrahydrofuran; water
T=80°C; 36 h; Schlenk techniqueInert atmosphere;
参考文献
Wang, Xingyong; Wang, Xiaodong; Liu, Miaochang; Ding, Jinchang; Chen, Jiuxi; Wu, Huayue
Synthesis (Germany), 2013 , vol. 45, # 16 art. no. SS-2013-F0255-OP, p. 2241 - 2244
反应条件
Mn(OAc)3•2H2O in ethanol
T=170°C; 0.166667 h; Microwave irradiation; regioselective reaction;
参考文献
Guchhait, Sankar K.; Kashyap, Maneesh; Saraf, Shuddham
Synthesis, 2010 , # 7 art. no. Z24009SS, p. 1166 - 1170
反应条件
potassium phosphate; palladium bis(2,2,6,6-tetramethyl-3,5-heptanedionate) in 1-methyl-pyrrolidin-2-one
T=125°C; 36 h;
参考文献
Nandurkar, Nitin S.; Bhanushali, Mayur J.; Bhor, Malhari D.; Bhanage, Bhalchandra M.
Tetrahedron Letters, 2008 , vol. 49, # 6 p. 1045 - 1048