2-苯基-1-苯并呋喃合成路线 （共 220 条）
反应条件
1,10-phenanthroline; Cu(acetate)2*(x)H2O; sodium acetate; palladium diacetate in 1,2-dichloro-ethane
T=110°C; 24 h; Molecular sieve;
参考文献
Sharma, Upendra; Naveen, Togati; Maji, Arun; Manna, Srimanta; Maiti, Debabrata
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12669 - 12673
Angew. Chem., 2013 , vol. 125, # 48 p. 12901 - 12905
反应条件
1,10-phenanthroline; Cu(acetate)2*(x)H2O; sodium acetate; palladium diacetate in 1,2-dichloro-ethane
T=110°C; 24 h; Molecular sieve;
参考文献
Sharma, Upendra; Naveen, Togati; Maji, Arun; Manna, Srimanta; Maiti, Debabrata
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12669 - 12673
Angew. Chem., 2013 , vol. 125, # 48 p. 12901 - 12905
反应条件
in water; acetonitrile
Irradiationvar. solvents ratio; pH 2 and pH 7; Quantum yield;
参考文献
Givens, Richard S.; Athey, Phillip S.; Kueper III, L. William; Matuszewski, Bogdan; Xue, Jie-You
Journal of the American Chemical Society, 1992 , vol. 114, # 22 p. 8708 - 8710
反应条件
1: With triethylamine in diethyl ether
T=0°C; Acylation; Heating;
2: With silica gel
Cyclization; aromatization;
参考文献
Ghosh, Somnath; Banerjee, Indira; Baul, Susmita
Tetrahedron, 1999 , vol. 55, # 38 p. 11537 - 11546
反应条件
copper(l) iodide; palladium; triphenylphosphine; aluminum oxide; potassium fluoride
Sonogashira coupling-cyclization; 0.0583333 h; microwave irradiation (100 percent power);
参考文献
Kabalka, George W.; Wang, Lei; Pagni, Richard M.
Tetrahedron, 2001 , vol. 57, # 38 p. 8017 - 8028
反应条件
1: 51 percent / sodium tert-butoxide / Pd2(dba)3; HP(tBu)3BF4 / dioxane / 9 h / 60 °C
2: 50 percent / sodium tert-butoxide / Pd2(dba)3; DPEphos / toluene / 100 °C
View Scheme
参考文献
Willis, Michael C.; Taylor, Dawn; Gillmore, Adam T.
Tetrahedron, 2006 , vol. 62, # 49 p. 11513 - 11520
反应条件
1: 51 percent / sodium tert-butoxide / Pd2(dba)3; HP(tBu)3BF4 / dioxane / 9 h / 60 °C
2: 50 percent / sodium tert-butoxide / Pd2(dba)3; DPEphos / toluene / 100 °C
View Scheme
参考文献
Willis, Michael C.; Taylor, Dawn; Gillmore, Adam T.
Tetrahedron, 2006 , vol. 62, # 49 p. 11513 - 11520
反应条件
1: 68 percent / bromine / CCl4 / Heating; Irradiation
2: 98 percent / toluene / 4 h / Heating
3: 82 percent / sodium t-amylate / toluene / Heating
View Scheme
参考文献
Hercouet, A.; Corre, M. Le
Tetrahedron, 1981 , vol. 37, # 16 p. 2867 - 2874
反应条件
potassium tert-butylate in tetrahydrofuran
T=80°C; 2 h; Inert atmosphere;
参考文献
Bochicchio, Antonella; Chiummiento, Lucia; Funicello, Maria; Lopardo, Maria Teresa; Lupattelli, Paolo
Tetrahedron Letters, 2010 , vol. 51, # 21 p. 2824 - 2827
反应条件
[2,2']bipyridinyl; para-nitrobenzenesulfonic acid; palladium diacetate in 2-methyl tetrahydrofuran; water
T=80°C; 36 h; Schlenk techniqueInert atmosphereGreen chemistry; Catalytic behavior; Reagent/catalystSolvent;
参考文献
Chen, Jiuxi; Li, Jianjun; Su, Weike
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 24 p. 4078 - 4083
