2-苯基-1-苯并呋喃合成路线 （共 220 条）
反应条件
1: 53 percent / palladium(II) acetate, triphenylphosphine / triethylamine / 4 h / 80 °C
2: 91 percent / lithium iodide / various solvent(s) / 18 h / Heating
View Scheme
参考文献
Buckle, Derek, R.; Rockell, Caroline J. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2443 - 2446
反应条件
toluene-4-sulfonic acid in dichloromethane
Reflux;
参考文献
Duan, Xin-Fang; Feng, Jian-Xia; Zhang, Zhan-Bin
Synthesis, 2010 , # 3 p. 515 - 519
反应条件
1: BF4(1-)*C54H36Au3Cl9OP3(1+) / tetrahydrofuran / 65 °C / Inert atmosphere
2: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate / tetrahydrofuran; water / 4.5 h / 60 °C / Inert atmosphere
View Scheme
参考文献
Chan, Julian M.W.; Amarante, Giovanni W.; Toste, F. Dean
Tetrahedron, 2011 , vol. 67, # 24 p. 4306 - 4312
反应条件
1: tetrabutyl ammonium fluoride / water
2: tetrabutyl ammonium fluoride; palladium diacetate; triphenylphosphine
View Scheme
参考文献
Liu, Jie; Chen, Wei; Ji, Yong; Wang, Lei
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1585 - 1592
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 100 °C
2: potassium tert-butylate / N,N-dimethyl-formamide / 6 h / |Inert atmosphere; |Reflux
View Scheme
参考文献
Chen, Wen; Deng, Xiao-Yan; Li, Yan; Yang, Li-Juan; Wan, Wei-Chao; Wang, Xue-Quan; Zhang, Hong-Bin; Yang, Xiao-Dong
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 15 p. 4297 - 4302
反应条件
1: acetonitrile / 2 h / 82 °C
2: triethylamine / toluene / 2 h / 110 °C
View Scheme
参考文献
Ferino, Giulio; Cadoni, Enzo; Matos, Maria Joao; Quezada, Elias; Uriarte, Eugenio; Santana, Lourdes; Vilar, Santiago; Tatonetti, Nicholas P.; Yanez, Matilde; Vina, Dolores; Picciau, Carmen; Serra, Silvia; Delogu, Giovanna
ChemMedChem, 2013 , vol. 8, # 6 p. 956 - 966
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 0.08 h / 25 °C
2: ethylenediamine / dichloromethane / 25 °C
3: hydrogen bromide / acetic acid / 6 h / |Reflux
View Scheme
参考文献
Ruan, Libo; Shi, Min; Mao, Shiwei; Yu, Lifang; Yang, Fan; Tang, Jie
Tetrahedron, 2014 , vol. 70, # 5 p. 1065 - 1070
反应条件
1: ethylenediamine / dichloromethane / 25 °C
2: hydrogen bromide / acetic acid / 6 h / |Reflux
View Scheme
参考文献
Ruan, Libo; Shi, Min; Mao, Shiwei; Yu, Lifang; Yang, Fan; Tang, Jie
Tetrahedron, 2014 , vol. 70, # 5 p. 1065 - 1070
反应条件
palladium diacetate; dimethyl sulfoxide
T=35°C; Sonogashira Cross-Coupling; 0.5 h;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 598 - 605
反应条件
sodium hydroxide; ethanol; water
T=195°C; im geschlossenen Rohr;
参考文献
Stoermer; Reuter
Chemische Berichte, 1903 , vol. 36, p. 3981
