2-苯基-1-苯并呋喃合成路线 (共 220 条)
反应条件
hydrogen bromide in acetic acid
6 h; Reflux; SolventReagent/catalystTemperatureTime;
参考文献
Ruan, Libo; Shi, Min; Mao, Shiwei; Yu, Lifang; Yang, Fan; Tang, Jie
Tetrahedron, 2014 , vol. 70, # 5 p. 1065 - 1070
反应条件
lithium iodide in various solvent(s)
18 h; Heating;
参考文献
Buckle, Derek, R.; Rockell, Caroline J. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2443 - 2446
反应条件
PdBr2(bipy)*DMSO; silver carbonate in 1,4-dioxane
T=150°C; 13 h; Inert atmosphere;
参考文献
Yanagisawa, Shuichi; Itami, Kenichiro
Tetrahedron, 2011 , vol. 67, # 24 p. 4425 - 4430
反应条件
1: With n-butyllithium in diethyl ether; hexane
T=0 - 20°C; 30 h;
2: With zinc(II) chloride in toluene
T=120°C; 1 h;
3: With ammonium chloride in water; toluene
参考文献
Nakamura, Masaharu; Ilies, Laurean; Otsubo, Saika; Nakamura, Eiichi
Organic Letters, 2006 , vol. 8, # 13 p. 2803 - 2805
反应条件
1-tert-butyl-4,4,4-tris(dimethylamino)-2,2-bis[tris(dimethylamino)-phosphoranylidenamino]-2Λ54Λ5-catenadi(phosphazene) in benzene
Cyclization; 14 h; Heating;
参考文献
Kraus, George A.; Zhang, Ning; Verkade, John G.; Nagarajan, Muthukaman; Kisanga, Philip B.
Organic Letters, 2000 , vol. 2, # 16 p. 2409 - 2410
反应条件
[bis(acetoxy)iodo]benzene in acetonitrile
T=20°C; 2 h; Inert atmosphere;
参考文献
Singh, Fateh V.; Wirth, Thomas
Synthesis, 2012 , vol. 44, # 8 p. 1171 - 1177
反应条件
tetra-butylammonium acetate; Pd EnCat-30TM in ethanol
T=120°C; Suzuki cross-coupling; 0.166667 h; microwave irradiation;
参考文献
Nun, Pierrick; Martinez, Jean; Lamaty, Frederic
Synlett, 2009 , # 11 p. 1761 - 1764
反应条件
[2,2']bipyridinyl; potassium carbonate; tris(dibenzylideneacetone)dipalladium (0) in acetonitrile
T=50°C; 5 h;
参考文献
Hu, Youhong; Nawoschik, Kenneth J.; Liao, Yun; Ma, Jian; Fathi, Reza; Yang, Zhen
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2235 - 2239
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride in 1,4-dioxane
T=70°C; 20 h;
参考文献
Khan, M. Wahab; Alam, M. Jahangir; Rashid; Chowdhury
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 16 p. 4796 - 4805
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; IPr*HBF4 in o-xylene
24 h; HeatingInert atmosphere;
参考文献
Farago, Janos; Kotschy, Andras
Synthesis, 2009 , # 1 p. 85 - 90