2-苯基-1-苯并呋喃合成路线 (共 220 条)
反应条件
toluene-4-sulfonic acid in ethanol
T=170°C; microwave irradiation;
参考文献
Jacubert, Maud; Hamze, Abdallah; Provot, Olivier; Peyrat, Jean-Francois; Brion, Jean-Daniel; Alami, Mouad
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3588 - 3592
反应条件
1: 2-(gem-dibromovinyl)phenol With tetrabutyl ammonium fluoride in N,N-dimethyl-formamide
T=20°C; 4 h; Sealed tubeInert atmosphere;
2: benzenesulphinic acid sodium salt With copper diacetate; triethylamine; palladium dichloride in N,N-dimethyl-formamide
T=110°C; 12 h; Sealed tubeInert atmosphere;
参考文献
Chen, Wei; Li, Pinhua; Miao, Tao; Meng, Ling-Guo; Wang, Lei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 3 p. 420 - 424
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in N,N-dimethyl-formamide
T=90°C; 4 h; Inert atmosphereSchlenk technique; Reagent/catalystConcentrationTimeSolvent; chemoselective reaction;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
European Journal of Organic Chemistry, 2013 , # 4 p. 781 - 788
反应条件
t-Bu-BippyPhos; tris-(dibenzylideneacetone)dipalladium(0); cesium hydroxide monohydrate in 1,4-dioxane
T=110°C; 12 h; Inert atmosphereGloveboxSealed tube;
参考文献
Lavery, Christopher B.; Rotta-Loria, Nicolas L.; McDonald, Robert; Stradiotto, Mark
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 5 p. 981 - 987
反应条件
t-Bu-BippyPhos; tris-(dibenzylideneacetone)dipalladium(0); cesium hydroxide monohydrate in 1,4-dioxane
T=110°C; 12 h; Inert atmosphereGloveboxSealed tube;
参考文献
Lavery, Christopher B.; Rotta-Loria, Nicolas L.; McDonald, Robert; Stradiotto, Mark
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 5 p. 981 - 987
反应条件
in acetonitrile
Irradiation;
参考文献
Givens, Richard S.; Athey, Phillip S.; Matuszewski, Bogdan; Kueper III, L. William; Xue, Jie-You; Fister, Thomas
Journal of the American Chemical Society, 1993 , vol. 115, # 14 p. 6001 - 6012
反应条件
Ti/C in tetrahydrofuran
参考文献
Fuerstner, Alois; Jumbam, Denis N.
Tetrahedron, 1992 , vol. 48, # 29 p. 5991 - 6010
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in N,N-dimethyl-formamide
T=100°C; Suzuki coupling;
参考文献
Chen, Wei; Zhang, Yicheng; Zhang, Lei; Wang, Min; Wang, Lei
Chemical Communications, 2011 , vol. 47, # 37 p. 10476 - 10478
反应条件
cyclopentene in toluene
T=100°C; 8 h; Inert atmosphere; regioselective reaction;
参考文献
Lee, Dong-Hwan; Kwon, Ki-Hyeok; Yi, Chae S.
Journal of the American Chemical Society, 2012 , vol. 134, # 17 p. 7325 - 7328
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium tert-butylate; silica gel in dimethyl sulfoxide
T=20 - 110°C; 0.05 h; Inert atmosphereMicrowave irradiation;
参考文献
Wu, Liansheng; Shi, Xiaokang; Xu, Xiaoyun; Liang, Fen; Huang, Guosheng
Journal of Chemical Sciences, 2011 , vol. 123, # 5 p. 697 - 702