2-苯基-1-苯并呋喃合成路线 (共 220 条)
反应条件
palladium diacetate in tetrahydrofuran
T=60°C; 24 h; TemperatureTime;
参考文献
Yang, Qi; Chang, Jiao; Wu, Qun; Zhang, Bianxiang
Research on Chemical Intermediates, 2012 , vol. 38, # 7 p. 1335 - 1340
反应条件
[2,2']bipyridinyl; palladium (II) trifluoroacetate; water; trifluoroacetic acid in tetrahydrofuran
T=80°C; 36 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Xingyong; Liu, Miaochang; Xu, Long; Wang, Qingzong; Chen, Jiuxi; Ding, Jinchang; Wu, Huayue
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5273 - 5281
反应条件
bis(η3-allyl-μ-chloropalladium(II)); N,N,N′,N′-tetra(diphenylphosphinomethyl)pyridine-2,6-diamine; caesium carbonate in N,N-dimethyl-formamide
T=130°C; Sonogashira Cross-Coupling; 9 h; Schlenk techniqueInert atmosphere; Reagent/catalystSolvent;
参考文献
Zhou, Rong; Wang, Wei; Jiang, Zhi-Jie; Wang, Kun; Zheng, Xue-Li; Fu, Hai-Yan; Chen, Hua; Li, Rui-Xiang
Chemical Communications, 2014 , vol. 50, # 45 p. 6023 - 6026
反应条件
1: iodobenzene; trimethylsilylacetylene With copper(l) iodide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride
T=80°C; Sonogashira coupling;
2: O-triisopropylsilyl-2-iodophenol With copper(l) iodide; tetrabutyl ammonium fluoride; bis-triphenylphosphine-palladium(II) chloride
T=80°C; Sonogashira coupling; Further stages.;
参考文献
Csekei, Marton; Novak, Zoltan; Kotschy, Andras
Tetrahedron, 2008 , vol. 64, # 37 p. 8992 - 8996
反应条件
N,N'-dibenzyl-BINAM; copper(II) bis(trifluoromethanesulfonate); potassium carbonate in 1,4-dioxane
T=110°C; 55 h; Inert atmosphere;
参考文献
Jaseer; Prasad; Sekar, Govindasamy
Tetrahedron, 2010 , vol. 66, # 11 p. 2077 - 2082
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran; hexane; pentane
T=20°C; 2.5 h; Inert atmosphere; regioselective reaction;
参考文献
Truong, Thanh; Daugulis, Olafs
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4243 - 4245
反应条件
[Pd(dppp)(H2O)2](BF4)2 in tetrahydrofuran
T=45°C; Molecular sieve;
参考文献
Wang, Huan; Han, Xiuling; Lu, Xiyan
Synlett, 2011 , # 17 p. 2590 - 2594
反应条件
[Pd(dppp)(H2O)2](BF4)2 in tetrahydrofuran
T=45°C; 2.5 h; Molecular sieve;
参考文献
Wang, Huan; Han, Xiuling; Lu, Xiyan
Synlett, 2011 , # 17 p. 2590 - 2594
反应条件
[Pd(dppp)(H2O)2](BF4)2 in tetrahydrofuran
T=45°C; Molecular sieve;
参考文献
Wang, Huan; Han, Xiuling; Lu, Xiyan
Synlett, 2011 , # 17 p. 2590 - 2594
反应条件
[Pd(dppp)(H2O)2](BF4)2 in tetrahydrofuran
T=45°C; Molecular sieve;
参考文献
Wang, Huan; Han, Xiuling; Lu, Xiyan
Synlett, 2011 , # 17 p. 2590 - 2594