2-苯基-1-苯并呋喃合成路线 (共 220 条)
反应条件
[Pd(dppp)(H2O)2](BF4)2 in tetrahydrofuran
T=45°C; Molecular sieve;
参考文献
Wang, Huan; Han, Xiuling; Lu, Xiyan
Synlett, 2011 , # 17 p. 2590 - 2594
反应条件
[Pd(dppp)(H2O)2](BF4)2 in tetrahydrofuran
T=45°C; Molecular sieve;
参考文献
Wang, Huan; Han, Xiuling; Lu, Xiyan
Synlett, 2011 , # 17 p. 2590 - 2594
反应条件
[Pd(dppp)(H2O)2](BF4)2 in tetrahydrofuran
T=45°C; Molecular sieve;
参考文献
Wang, Huan; Han, Xiuling; Lu, Xiyan
Synlett, 2011 , # 17 p. 2590 - 2594
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; triphenylphosphine in 1-methyl-pyrrolidin-2-one
T=80°C; tandem elimination-addition-Hiyama coupling; 12 h;
参考文献
Liu, Jie; Chen, Wei; Ji, Yong; Wang, Lei
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1585 - 1592
反应条件
5 palladium on charcoal in ethanol
T=60°C; 22 h; regioselective reaction;
参考文献
Tang, Dan-Tam D.; Collins, Karl D.; Ernst, Johannes B.; Glorius, Frank
Angewandte Chemie - International Edition, 2014 , vol. 53, # 7 p. 1809 - 1813
Angew. Chem., 2014 , vol. 126, # 07 p. 1840 - 1844,5
反应条件
toluene-4-sulfonic acid in toluene
3 h; Heating;
参考文献
Hercouet, A.; Corre, M. Le
Tetrahedron, 1981 , vol. 37, # 16 p. 2867 - 2874
反应条件
1: 2,3-benzofuran With n-butyllithium in tetrahydrofuran; hexane
T=-10°C; 1 h;
2: o-di-fluorobenzene in tetrahydrofuran; hexane
T=20 - 60°C; 13 h;
参考文献
Becht, Jean-Michel; Gissot, Arnaud; Wagner, Alain; Mioskowski, Charles
Chemistry - A European Journal, 2003 , vol. 9, # 14 p. 3209 - 3215
反应条件
1: aq. HCl / tetrahydrofuran; propan-2-ol / 20 °C
2: 97 percent / PtCl2 / toluene / 1.5 h / 80 °C
View Scheme
参考文献
Fuerstner, Alois; Davies, Paul W.
Journal of the American Chemical Society, 2005 , vol. 127, # 43 p. 15024 - 15025
反应条件
1: PdCl2(PPh3)2; CuI; Et3N / 50 °C
2: aq. HCl / tetrahydrofuran; propan-2-ol / 20 °C
3: 97 percent / PtCl2 / toluene / 1.5 h / 80 °C
View Scheme
参考文献
Fuerstner, Alois; Davies, Paul W.
Journal of the American Chemical Society, 2005 , vol. 127, # 43 p. 15024 - 15025
反应条件
1: 90 percent / Et3N; PdCl2(PPh3)2; CuI / dioxane / 20 °C
2: 85 percent / KF/Al2O3 / 0.05 h / microwave irradiation (30 percent power)
3: 56 percent / PPh3; CuI; Pd / KF/Al2O3 / 0.06 h / microwave irradiation (100 percent power)
View Scheme
参考文献
Kabalka, George W.; Wang, Lei; Pagni, Richard M.
Tetrahedron, 2001 , vol. 57, # 38 p. 8017 - 8028