3-氧代-2-苯基-4,4,5,5-四甲基咪唑啉-1-氧合成路线 （共 10 条）
反应条件
sodium periodate in chloroform; water T=0 - 20°C;
参考文献
Rajca, Andrzej; Pink, Maren; Mukherjee, Sumit; Rajca, Suchada; Das, Kausik
Tetrahedron, 2007 , vol. 63, # 44 p. 10731 - 10742
反应条件
1: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid in dichloromethane 1 h; Ice cooling; 2: With sodium periodate in dichloromethane Further stages.;
参考文献
Chemistry - A European Journal, , vol. 7, # 9 p. 2007 - 2014
反应条件
1: 79 percent / Al/Hg / tetrahydrofuran; H2O / 0.75 h / -7 - -2 °C 2: 96 percent / p-TsOH*H2O / methanol / 48 h / 20 °C 3: 85 percent / NaIO4 / CHCl3; H2O / 0 - 20 °C View Scheme
参考文献
Tetrahedron, , vol. 63, # 44 p. 10731 - 10742
反应条件
sodium tungstate; dihydrogen peroxide in methanol 48 h; Ambient temperature;
参考文献
Kalai, Tamas; Jeko, Jozsef; Szabo, Zoltan; Parkanyi, Laszlo; Hideg, Kalman
Synthesis, 1997 , # 9 p. 1049 - 1055
反应条件
1: 96 percent / p-TsOH*H2O / methanol / 48 h / 20 °C 2: 85 percent / NaIO4 / CHCl3; H2O / 0 - 20 °C View Scheme
参考文献
Tetrahedron, , vol. 63, # 44 p. 10731 - 10742
反应条件
1.1: 78 percent / aq. H2SO4 / methanol / 1 h / 20 °C / pH 3 - 4 2.1: m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 / 1 h / Ice cooling 2.2: 78 percent / aq. NaIO4 / CH2Cl2 View Scheme
参考文献
Chemistry - A European Journal, , vol. 7, # 9 p. 2007 - 2014
反应条件
hydrogenchloride; sodium nitrite in 1,4-dioxane 0.25 h; Ambient temperature;
参考文献
Kalai, Tamas; Jeko, Jozsef; Szabo, Zoltan; Parkanyi, Laszlo; Hideg, Kalman
Synthesis, 1997 , # 9 p. 1049 - 1055
反应条件
1: With 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in methanol T=20°C; 2: With lead dioxide in methanol 1 h;
参考文献
Fursova, Elena Yu.; Ovcharenko, Victor I.; Romanenko, Galina V.; Tretyakov, Eugene V.
Tetrahedron Letters, 2003 , vol. 44, # 34 p. 6397 - 6399
反应条件
hydrogenchloride; zinc
T=100°C; 1.5 h;
参考文献
Kalai, Tamas; Jeko, Jozsef; Szabo, Zoltan; Parkanyi, Laszlo; Hideg, Kalman
Synthesis, 1997 , # 9 p. 1049 - 1055
反应条件
iron; acetic acid
1 h; Ambient temperature;
参考文献
Kalai, Tamas; Jeko, Jozsef; Szabo, Zoltan; Parkanyi, Laszlo; Hideg, Kalman
Synthesis, 1997 , # 9 p. 1049 - 1055
