5,6-二溴-2,1,3-苯并噻二唑合成路线 （共 6 条）
反应条件
thionyl chloride; triethylamine in dichloromethane 5 h; Cooling with iceReflux;
参考文献
Shao, Jinjun; Chang, Jingjing; Chi, Chunyan
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 35 p. 7045 - 7052
反应条件
1: 89 percent / Br2, acetic acid, sodium acetate 2: 83.5 percent / sulfuric acid 3: 76 percent / thionyl chloride, pyridine / 3 h / Heating View Scheme
参考文献
Shao, Jinjun; Chang, Jingjing; Chi, Chunyan
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 35 p. 7045 - 7052
反应条件
1: 83.5 percent / sulfuric acid 2: 76 percent / thionyl chloride, pyridine / 3 h / Heating View Scheme
参考文献
Shao, Jinjun; Chang, Jingjing; Chi, Chunyan
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 35 p. 7045 - 7052
反应条件
1: 87 percent / pyridine 2: 89 percent / Br2, acetic acid, sodium acetate 3: 83.5 percent / sulfuric acid 4: 76 percent / thionyl chloride, pyridine / 3 h / Heating View Scheme
参考文献
Shao, Jinjun; Chang, Jingjing; Chi, Chunyan
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 35 p. 7045 - 7052
反应条件
(i) H2, Raney-Ni, THF, (ii) PhNSO, toluene; Multistep reaction;
参考文献
Moerkved, Eva H.; Neset, Siren M.; Bjoerlo, Olav; Kjoesen, Helge; Hvistendahl, Georg; Mo, Frode
Acta Chemica Scandinavica, 1995 , vol. 49, # 9 p. 658 - 662
反应条件
1: 35 percent / HNO3, H2SO4 / 10 h / Heating 2: 100 percent / Sn, HCl / ethanol 3: 76 percent / thionyl chloride, pyridine / 3 h / Heating View Scheme
参考文献
Moerkved, Eva H.; Neset, Siren M.; Bjoerlo, Olav; Kjoesen, Helge; Hvistendahl, Georg; Mo, Frode
Acta Chemica Scandinavica, 1995 , vol. 49, # 9 p. 658 - 662
