(癸基氧基)(三甲基)硅烷合成路线 (共 12 条)
反应条件
Aliquatreg; 336; potassium carbonate in Petroleum ether T=60°C; 4 h;
参考文献
Lissel, M.; Weiffen, J
Synthetic Communications, 1981 , vol. 11, # 7 p. 545 - 550
反应条件
montmorillonite K-10 in dichloromethane 0.4 h; Ambient temperature;
参考文献
Jin, Tong-Shou; Tian, Ruo-Fei; Liu, Li-Bin; Zhao, Ying; Li, Tong-Shuang
Synthetic Communications, 2006 , vol. 36, # 13 p. 1823 - 1828
反应条件
chloro-trimethyl-silane T=65 - 150°C; 3 h;
参考文献
Millar, Ross W.; Philbin, Simon P.
Tetrahedron, 1997 , vol. 53, # 12 p. 4371 - 4386
反应条件
in acetonitrile T=100°C; 2 h;
参考文献
Horibe; Oshita
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 1 p. 181 - 182
参考文献
Knausz, Dezsoe; Meszticzky, Aranka; Szakacs, Laszlo; Csakvari, Bela; Ujszaszy, Kalman
Journal of Organometallic Chemistry, 1983 , vol. 256, # 1 p. 11 - 22
反应条件
Sn-clay montmorrillonite in dichloromethane T=30°C; 0.166667 h; other ion-exchanged clay montmorrillonites;
参考文献
Onaka, Makoto; Hosokawa, Yasutaka; Higuchi, Katsumi; Izumi, Yusuke
Tetrahedron Letters, 1993 , vol. 34, # 7 p. 1171 - 1172
参考文献
Woronkow; Schabarowa
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 1528,1530;engl.Ausg.S.1501,1503
参考文献
Gordetsov,A.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1977 , vol. 47, # 2 p. 372 - 376,345 - 349
反应条件
dinitrogen pentaoxide in dichloromethane T=-5 - 8°C; 1.5 h;
参考文献
Millar, Ross W.; Philbin, Simon P.
Tetrahedron, 1997 , vol. 53, # 12 p. 4371 - 4386
反应条件
toluene-4-sulfonic acid in n-heptane T=60°C; 0.166667 h; Product distribution;
参考文献
Nedogrei, E. P.; Musavirov, R. C.; Zlomskii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 9 p. 2078 - 2081,1875 - 1877