1,2-二乙氧基-1,1,2,2-四甲基二硅烷合成路线 （共 13 条）
反应条件
1: para-iodoanisole With N-ethyl-N,N-diisopropylamine; palladium dichloride; biphenyl-2-yl-di-tert-butyl-phosphane in 1-methyl-pyrrolidin-2-one T=20°C; 0.5 h; 2: 1,2-diethoxy-1,1,2,2-tetramethyldisilane in dichloromethane T=20°C; 48 h;
参考文献
Organic Letters, , vol. 5, # 19 p. 3483 - 3486
反应条件
1: 1-bromo-4-methoxy-benzene With N-ethyl-N,N-diisopropylamine; palladium dichloride; biphenyl-2-yl-di-tert-butyl-phosphane in 1-methyl-pyrrolidin-2-one T=20°C; 0.166667 h; 2: 1,2-diethoxy-1,1,2,2-tetramethyldisilane in dichloromethane T=60°C; 10 h;
参考文献
Organic Letters, , vol. 5, # 19 p. 3483 - 3486
反应条件
hydrogen fluoride; water
参考文献
Kumada et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 1264,1267
