N-苯基-1,3-苯并噻唑-2-胺合成路线 (共 75 条)
反应条件
1: (i) aq. HCl, aq. NaNO2, (ii) /BRN= 1718733/, (reflux)
2: aq. HCl
3: CH2Cl2 / Heating
View Scheme
参考文献
Takahashi,S. et al.
Chemical and Pharmaceutical Bulletin, 1970 , vol. 18, p. 1176 - 1184
反应条件
in 1,4-dioxane
T=90°C; 64 h;
参考文献
Morita, Hiroyuki; Tashiro, Shintaro; Takeda, Masahiro; Yamada, Nobuhiko; Sheikh, Md. Chanmiya; Kawaguchi, Hiroyuki
Tetrahedron, 2008 , vol. 64, # 19 p. 4496 - 4505
反应条件
1: aq. HCl / Heating
2: CH2Cl2 / Heating
View Scheme
参考文献
Takahashi,S. et al.
Chemical and Pharmaceutical Bulletin, 1970 , vol. 18, p. 1176 - 1184
反应条件
1: CHCl3
2: AcOH
3: Zn, AcOH
View Scheme
参考文献
Kresze,G. et al.
Justus Liebigs Annalen der Chemie, 1968 , vol. 715, p. 223 - 237
反应条件
1: neat (no solvent)
2: potassium carbonate / water / 10 h / 100 °C / |Green chemistry
View Scheme
参考文献
Rout, Saroj Kumar; Guin, Srimanta; Nath, Jayashree; Patel, Bhisma K.
Green Chemistry, 2012 , vol. 14, # 9 p. 2491 - 2498
反应条件
1: neat (no solvent)
2: potassium carbonate / water / 8 h / 100 °C / |Green chemistry
View Scheme
参考文献
Rout, Saroj Kumar; Guin, Srimanta; Nath, Jayashree; Patel, Bhisma K.
Green Chemistry, 2012 , vol. 14, # 9 p. 2491 - 2498
反应条件
1: neat (no solvent)
2: potassium carbonate / water / 33 h / 100 °C / |Green chemistry
View Scheme
参考文献
Rout, Saroj Kumar; Guin, Srimanta; Nath, Jayashree; Patel, Bhisma K.
Green Chemistry, 2012 , vol. 14, # 9 p. 2491 - 2498
反应条件
1: neat (no solvent)
2: potassium carbonate / water / 43 h / 100 °C / |Green chemistry
View Scheme
参考文献
Rout, Saroj Kumar; Guin, Srimanta; Nath, Jayashree; Patel, Bhisma K.
Green Chemistry, 2012 , vol. 14, # 9 p. 2491 - 2498
反应条件
in methanol; chloroform
45 h; Irradiation;
参考文献
Muthusamy, Sengoden; Paramasivam, Rangasamy; Ramakrishnan, Vayalakkavoor T.
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 3 p. 759 - 763
反应条件
in methanol; chloroform
45 h; Irradiation;
参考文献
Muthusamy, Sengoden; Paramasivam, Rangasamy; Ramakrishnan, Vayalakkavoor T.
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 3 p. 759 - 763