5-异丁基四氢呋喃-2-酮合成路线 （共 6 条）
反应条件
in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
Zultanski, Susan L.; Fu, Gregory C.
Journal of the American Chemical Society, 2011 , vol. 133, # 39 p. 15362 - 15364
反应条件
sulfuric acid in water T=100°C; 48 h;
参考文献
Patel, Nandini C.; Schwarz, Jacob B.; Islam, Khondaker; Miller, Whitney; Tran, Tuan P.; Wei, Yunjing
Synthetic Communications, 2011 , vol. 41, # 15 p. 2209 - 2215
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 16 h / 20 °C 2: sulfuric acid / water / 48 h / 100 °C View Scheme
参考文献
Patel, Nandini C.; Schwarz, Jacob B.; Islam, Khondaker; Miller, Whitney; Tran, Tuan P.; Wei, Yunjing
Synthetic Communications, 2011 , vol. 41, # 15 p. 2209 - 2215
反应条件
hydrogen bromide; copper (I) cyanide anschliessende Behandlung mit wss. Schwefelsaeure;
参考文献
Darzens
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 288, p. 185
反应条件
boron trifluoride diethyl etherate; water; naphthalenyllithium; 3-chloro-benzenecarboperoxoic acid 1.) THF, -78 deg C, 6 h, 2.) 20 deg C, 2 h, 3.) CH2Cl2; Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Fernandez, Jose R.; Rubiera, Covadonga; Yus, Miguel
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3113 - 3118
参考文献
Fromm; Lischke
Chemische Berichte, 1900 , vol. 33, p. 1203
