3,6-二甲基-2-丙基吡嗪合成路线 （共 11 条）
反应条件
1: propyl bromide With iron (III) acetylacetonate; magnesium in tetrahydrofuran 2: 3-chloro-2,5-dimethyl-pyrazine With 1-methyl-pyrrolidin-2-one T=0°C; 0.25 h;
参考文献
Dickschat, Jeroen S.; Wickel, Susanne; Bolten, Christoph J.; Nawrath, Thorben; Schulz, Stefan; Wittmann, Christoph
European Journal of Organic Chemistry, 2010 , # 14 p. 2687 - 2695
反应条件
in toluene T=300°C; Yield given;
参考文献
Buechi, George; Galindo, Jose
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2605 - 2606
反应条件
1: 73 percent / isoamyl nitrite, conc. HCl / diethyl ether / 2 h / 10 - 20 °C 2: 93 percent / hexane / Heating 3: potassium tert-butoxide / dimethylsulfoxide / 2 h / 50 °C 4: Et3N / CH2Cl2 / 10 - 20 °C 5: toluene / 300 °C View Scheme
参考文献
Buechi, George; Galindo, Jose
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2605 - 2606
反应条件
1: 93 percent / hexane / Heating 2: potassium tert-butoxide / dimethylsulfoxide / 2 h / 50 °C 3: Et3N / CH2Cl2 / 10 - 20 °C 4: toluene / 300 °C View Scheme
参考文献
Buechi, George; Galindo, Jose
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2605 - 2606
反应条件
1: potassium tert-butoxide / dimethylsulfoxide / 2 h / 50 °C 2: Et3N / CH2Cl2 / 10 - 20 °C 3: toluene / 300 °C View Scheme
参考文献
Buechi, George; Galindo, Jose
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2605 - 2606
反应条件
1: Et3N / CH2Cl2 / 10 - 20 °C 2: toluene / 300 °C View Scheme
参考文献
Buechi, George; Galindo, Jose
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2605 - 2606
参考文献
Wheeler, J. W.; Avery, J.; Olubajo, O.; Shamim, M. T.; Strom, C. B.; Duffield, R. M.
Tetrahedron, 1982 , vol. 38, # 13 p. 1939 - 1948
反应条件
in water T=130°C; Maillard reaction; pH=8; 2 h;
参考文献
Van Lancker, Fien; Adams; De Kimpe, Norbert
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 4 p. 2470 - 2478
反应条件
in water T=130°C; Maillard reaction; pH=8; 2 h;
参考文献
Van Lancker, Fien; Adams; De Kimpe, Norbert
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 4 p. 2470 - 2478
反应条件
in water T=130°C; Maillard reaction; pH=8; 2 h;
参考文献
Van Lancker, Fien; Adams; De Kimpe, Norbert
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 4 p. 2470 - 2478
