N,N-二甲基吡啶-3-胺合成路线 （共 9 条）
反应条件
NHC-Pd(II)-Im; potassium tert-butylate in tetrahydrofuran T=20°C; 6 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 20 p. 9236 - 9239,4
Journal of Organic Chemistry, , vol. 77, # 20 p. 9236 - 9239
反应条件
NHC-Pd(II)-Im; potassium tert-butylate in tetrahydrofuran T=20°C; 6 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 20 p. 9236 - 9239,4
Journal of Organic Chemistry, , vol. 77, # 20 p. 9236 - 9239
反应条件
in formic acid Alkylation; Heating;
参考文献
Synthetic Communications, , vol. 29, # 19 p. 3341 - 3352
反应条件
tripotassium phosphate monohydrate; chloro(2-dicyclohexylphosphino-2',4',6'-triisopropyl-1,1'-biphenyl)[2-(2'-amino-1,1'-biphenyl)]palladium(II) in tetrahydrofuran T=110°C; 16 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 50, # 26 p. 3672 - 3674
反应条件
aluminum oxide; pumice stone T=380 - 420°C;
参考文献
Roczniki Chemii, , vol. 14, p. 326,330
Chem. Zentralbl., , vol. 106, # I p. 70
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 4935 - 4953
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 4935 - 4953
反应条件
1: 3-(N,N-dimethylamino)-pyridine With boron trifluoride diethyl etherate in tetrahydrofuran T=0°C; 0.5 h; 2: With lithium diisopropyl amide in tetrahydrofuran; hexane T=-78°C; 0.5 h; 3: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 13 h;
参考文献
Felten, Albert E.; Zhu, Gangguo; Aron, Zachary D.
Organic Letters, 2010 , vol. 12, # 9 p. 1916 - 1919
反应条件
2,4,4,6-tetrabromo-2,5-cyclohexadien-1-one
Bromination;
参考文献
Janiak, Christoph; Deblon, Stephan; Wu, He-Ping
Synthetic Communications, 1999 , vol. 29, # 19 p. 3341 - 3352
