4-硝基苯基氨基甲酸叔丁酯合成路线 (共 23 条)
反应条件
in ethylene glycol dimethyl ether T=-10°C;
参考文献
Saito, Yukako; Ouchi, Hidekazu; Takahata, Hiroki
Tetrahedron, 2006 , vol. 62, # 50 p. 11599 - 11607
反应条件
in tert-butyl alcohol T=20°C; 3 h;
参考文献
Strazzolini, Paolo; Melloni, Tiziana; Giumanini, Angelo G
Tetrahedron, 2001 , vol. 57, # 43 p. 9033 - 9043
反应条件
1: 2-methyl-propan-2-ol / 3 h / 20 °C 2: 86 percent / HNO3 / CH2Cl2 / 2 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 57, # 43 p. 9033 - 9043
参考文献
Journal of Organic Chemistry, , vol. 40, p. 3554 - 3561
反应条件
1: 86 percent / hexane / 8 h / 20 °C 2: 38 percent / 1,2-dimethoxy-ethane / -10 °C View Scheme
参考文献
Tetrahedron, , vol. 62, # 50 p. 11599 - 11607
反应条件
diphenyl phosphoryl azide; triethylamine
参考文献
Tetrahedron, , vol. 30, p. 2151 - 2157
反应条件
in 2,2,4-trimethylpentane T=25°C; Rate constantEquilibrium constantMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 10 p. 1671 - 1674
反应条件
1) toluene, reflux, 0.5 h; 2) toluene, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 20 p. 2975 - 2982
反应条件
EPZG clay in dichloromethane deacylation; 1.5 h; Heating;
参考文献
Shaikh, Nadim S.; Gajare, Anil S.; Deshpande, Vishnu H.; Bedekar, Ashutosh V.
Tetrahedron Letters, 2000 , vol. 41, # 3 p. 385 - 387
反应条件
hydrogen; palladium 10 on activated carbon in ethyl acetate 16 h;
参考文献
LEGOCHEM BIOSCIENCE LTD.
Patent: US2011/112083 A1, 2011 ;
Location in patent: Page/Page column 15 ;