4-甲氧基苯基氨基甲酸叔丁酯合成路线 （共 34 条）
反应条件
triethylamine; palladium dichloride in N,N-dimethyl acetamide T=70°C; P=760.051 Torr; 24 h; Schlenk technique;
参考文献
Ren, Long; Jiao, Ning
Chemical Communications, 2014 , vol. 50, # 28 p. 3706 - 3709
反应条件
1: 4-MeOC6H4Li With zinc(II) chloride in diethyl ether; hexane T=0°C; 0.5 h; Inert atmosphere; 2: N-(tert-butoxycarbonyl)-3-(4-cyanophenyl)-oxaziridine in diethyl ether; hexane T=0°C; 1.5 h; Inert atmosphere;
参考文献
Ghoraf, Mohammed; Vidal, Joelle
Tetrahedron Letters, 2008 , vol. 49, # 52 p. 7383 - 7385
反应条件
t-Bu Brett Phos; C44H62NO5PPdS; caesium carbonate in 1,4-dioxane T=50°C; 20 h; Sealed tubeInert atmosphere;
参考文献
Cheung, Chi Wai; Buchwald, Stephen L.
Organic Letters, 2013 , vol. 15, # 15 p. 3998 - 4001
反应条件
1: 4-nitrophenylsulfonyl chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 0 °C / |Inert atmosphere 2: 1-methyl-1H-imidazole / acetonitrile / 3 h / 23 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 3 p. 602 - 605
反应条件
1: acetonitrile / 1 h / 20 °C 2: hydroxylamine / acetonitrile; water / 14 h / 23 °C 3: 4-nitrophenylsulfonyl chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 0 °C / |Inert atmosphere 4: 1-methyl-1H-imidazole / acetonitrile / 3 h / 23 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 3 p. 602 - 605
反应条件
1: hydroxylamine / acetonitrile; water / 14 h / 23 °C 2: 4-nitrophenylsulfonyl chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 0 °C / |Inert atmosphere 3: 1-methyl-1H-imidazole / acetonitrile / 3 h / 23 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 3 p. 602 - 605
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane 0.5 h;
参考文献
Wild, Gareth. P.; Wiles, Charlotte; Watts, Paul; Haswell, Stephen J.
Tetrahedron, 2009 , vol. 65, # 8 p. 1618 - 1629
反应条件
1: sodium azide; copper(II) sulfate / methanol / 12 h / 30 °C 2: palladium dichloride; triethylamine / N,N-dimethyl acetamide / 24 h / 70 °C / 760.05 Torr / |Schlenk technique View Scheme
参考文献
Chemical Communications, , vol. 50, # 28 p. 3706 - 3709
反应条件
1: 86 percent / NaH / tetrahydrofuran 2: 1.) n-BuLi, (-)-sparteine / 1.) toluene, -78 deg C, 4 h, 2.) toluene, -78 deg C -> room temperature 3: ammonium cerium(IV) nitrate / acetonitrile; H2O / 0.5 h / 0 °C View Scheme
参考文献
Kim, Bong Jin; Park, Yong Sun; Beak, Peter
Journal of Organic Chemistry, 1999 , vol. 64, # 5 p. 1705 - 1708
反应条件
water T=100°C; 6 h; Inert atmosphere;
参考文献
Wang, Jia; Liang, Yan-Liang; Qu, Jin
Chemical Communications, 2009 , # 34 p. 5144 - 5146
