HCl in acetic acid aq. acetic acid; addn. of concd. HCl to HReO4, addn. of soln. to phosphine in acetic acid, stirred for 1 h at ambient temp.; filtered, washed with acetic acid and ether, dried under vac.; elem. anal.;
参考文献
Detty, Michael R.; Jones, William D.
Journal of the American Chemical Society, 1987 , vol. 109, # 19 p. 5666 - 5673
in chloroform-d1 byproducts: MeP(O)(PPh)2; under N2; phosphine (5-100 equiv.) added to soln. of Pd complex in CDCl3at 25°C; 24 h; not isolated; monitored by (1)H and (31)P NMR spectra;
参考文献
Stockland Jr., Robert A.; Levine, Adam M.; Giovine, Matthew T.; Guzei, Ilia A.; Cannistra, Joseph C.
Organometallics, 2004 , vol. 23, # 4 p. 647 - 656
