1-氯-1-(2-苯基亚肼基)乙酮合成路线 （共 22 条）
反应条件
tetrabutylammomium bromide; potassium carbonate in benzene 0.5 h; Ambient temperature;
参考文献
Abramov, M. A.; Galishev, V. A.; Petrov, M. L.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 11.1 p. 1795 - 1804
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 11 p. 2162 - 2173
反应条件
1: 10.7 g / Et3N / ethanol / 2 h / Heating 2: 6.5 percent / PPA / 0.17 h / 95 °C 3: H2 / Pd/C 10percent / ethyl acetate / 38000 Torr / Ambient temperature View Scheme
参考文献
Benincori, Tiziana; Sannicolo, Franco
Journal of Organic Chemistry, 1988 , vol. 53, # 6 p. 1309 - 1312
反应条件
1: EtONa / ethanol / 0.5 h / Heating 2: 60 percent / polyphosphoric acid / 0.25 h / 110 °C View Scheme
参考文献
Benincori, Tiziana; Fusco, Raffaello; Sannicolo, Franco
Gazzetta Chimica Italiana, 1990 , vol. 120, # 10 p. 635 - 639
反应条件
sodium hydroxide in ethanol Ambient temperature;
参考文献
Zohdi, Hussein F.; Rateb, Nora M.; Abdelhamid, Abdou O.
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 133, p. 103 - 117
反应条件
sodium hydroxide in ethanol
Ambient temperature;
参考文献
Zohdi, Hussein F.; Rateb, Nora M.; Abdelhamid, Abdou O.
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 133, p. 103 - 117
反应条件
p-tolylmethylenecyanothioacetamide; triethylamine in ethanol
Ambient temperature;
参考文献
Zohdi, Hussein F.; Rateb, Nora M.; Abdelhamid, Abdou O.
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 133, p. 103 - 117
反应条件
sodium hydroxide in ethanol
Ambient temperature;
参考文献
Zohdi, Hussein F.; Rateb, Nora M.; Abdelhamid, Abdou O.
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 133, p. 103 - 117
反应条件
1: 66 percent / Et3N; aq. NaOH / tetrahydrofuran; methanol / 0 - 20 °C
2: 59 percent / tetrahydrofuran / 20 °C
View Scheme
参考文献
Eweiss, N.F.; Osman, A.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1713 - 1717
反应条件
triethylamine in ethanol
3 h; Heating;
参考文献
Abdelhamid, Abdou O.; Hassaneen, Hamdi M.; Shawali, Ahmad S.; Parkanyi, Cyril
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 639 - 644
反应条件
triethylamine in toluene
5 h; Reflux;
参考文献
Wang, Li-Ya; Tsai, Henry J.; Lin, Hui-Yi; Kaneko, Kimiyoshi; Cheng, Fen-Ying; Shih, Hsin-Siao; Wong, Fung Fuh; Huang, Jiann-Jyh
RSC Advances, 2014 , vol. 4, # 27 p. 14215 - 14220
