2-丁基-1,3-环己烷二酮合成路线 （共 13 条）
反应条件
L-proline in dichloromethane T=25°C; 0.5 h;
参考文献
Ramachary, Dhevalapally B.; Kishor, Mamillapalli
Journal of Organic Chemistry, 2007 , vol. 72, # 14 p. 5056 - 5068
反应条件
potassium tert-butylate in diethyl ether; tert-butyl alcohol 5 h; Heating;
参考文献
Carruthers, William; Cumming, S. Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2383 - 2386
反应条件
hydrogenchloride; water in acetone T=20°C;
参考文献
Poldy, Jacqueline; Peakall, Rod; Barrow, Russell Allan
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 20 p. 4296 - 4300
反应条件
sodium ethanolate; sodium; xylene
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1952 , vol. 72, p. 51,53
Chem.Abstr., 1952 , p. 11142
反应条件
1: sodium ethylate; ethanol 2: sodium ethylate; ethanol; benzene 3: aq.-ethanolic sulfuric acid 4: sodium; sodium ethylate; xylene View Scheme
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1952 , vol. 72, p. 51,53
Chem.Abstr., 1952 , p. 11142
反应条件
1: aq.-ethanolic sulfuric acid 2: sodium; sodium ethylate; xylene View Scheme
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1952 , vol. 72, p. 51,53
Chem.Abstr., 1952 , p. 11142
反应条件
1: sodium ethylate; ethanol; benzene 2: aq.-ethanolic sulfuric acid 3: sodium; sodium ethylate; xylene View Scheme
参考文献
Nakazawa; Matsuura
Yakugaku Zasshi, 1952 , vol. 72, p. 51,53
Chem.Abstr., 1952 , p. 11142
反应条件
potassium ethanolate
参考文献
Stetter; Dierichs
Chemische Berichte, 1952 , vol. 85, p. 61,71
反应条件
1: aqueous barium hydroxide solution 2: sodium; hydrazine hydrate; diethylene glycol View Scheme
参考文献
Stetter; Dierichs
Chemische Berichte, 1952 , vol. 85, p. 61,71
反应条件
1: 98 percent / toluene-p-sulphonic acid / benzene / 24 h / Heating
2: 1.) Mg, 1,2-dibromoethane / 1.) THF, -78 deg C, 30 min, 2.) room temperature, 15 h
3: 7.9 g / pyridinium toluene-p-sulphonate / ethanol / 5 h / 60 °C
View Scheme
参考文献
Carruthers, William; Cumming, S. Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2383 - 2386
