2-丁基-1,3-环己烷二酮合成路线 (共 13 条)
反应条件
1: 98 percent / toluene-p-sulphonic acid / benzene / 24 h / Heating
2: 1.) Mg, 1,2-dibromoethane / 1.) THF, -78 deg C, 30 min, 2.) room temperature, 15 h
View Scheme
参考文献
Carruthers, William; Cumming, S. Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2383 - 2386
反应条件
toluene-4-sulfonic acid in benzene
24 h; Heating;
参考文献
Carruthers, William; Cumming, S. Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2383 - 2386
参考文献
Stetter; Dierichs
Chemische Berichte, 1952 , vol. 85, p. 61,71