5-[[(1,1-二甲基乙氧基)羰基]氨基]-6-氧代-2-苯基-1(6h)-嘧啶乙酸合成路线 （共 3 条）
反应条件
sodium hydroxide in methanol T=20°C; 2 h;
参考文献
Ohmoto, Kazuyuki; Okuma, Motohiro; Yamamoto, Tetsuya; Kijima, Hideomi; Sekioka, Tomohiko; Kitagawa, Kanji; Yamamoto, Shigeki; Tanaka, Kenji; Kawabata, Kazuhito; Sakata, Atsushi; Imawaka, Haruo; Nakai, Hisao; Toda, Masaaki
Bioorganic and Medicinal Chemistry, 2001 , vol. 9, # 5 p. 1307 - 1323
反应条件
1: 1.83 g / diethyl ether; methanol / 0 °C 2: 95 percent / hydrogen; HCl / Pd-C / ethyl acetate; methanol / 2 h / 20 °C 3: 93 percent / tetrahydrofuran / 120 h / Heating 4: 1.07 g / sodium hydroxide / methanol / 2 h / 20 °C View Scheme
参考文献
Ohmoto, Kazuyuki; Okuma, Motohiro; Yamamoto, Tetsuya; Kijima, Hideomi; Sekioka, Tomohiko; Kitagawa, Kanji; Yamamoto, Shigeki; Tanaka, Kenji; Kawabata, Kazuhito; Sakata, Atsushi; Imawaka, Haruo; Nakai, Hisao; Toda, Masaaki
Bioorganic and Medicinal Chemistry, 2001 , vol. 9, # 5 p. 1307 - 1323
反应条件
1: 93 percent / tetrahydrofuran / 120 h / Heating 2: 1.07 g / sodium hydroxide / methanol / 2 h / 20 °C View Scheme
参考文献
Ohmoto, Kazuyuki; Okuma, Motohiro; Yamamoto, Tetsuya; Kijima, Hideomi; Sekioka, Tomohiko; Kitagawa, Kanji; Yamamoto, Shigeki; Tanaka, Kenji; Kawabata, Kazuhito; Sakata, Atsushi; Imawaka, Haruo; Nakai, Hisao; Toda, Masaaki
Bioorganic and Medicinal Chemistry, 2001 , vol. 9, # 5 p. 1307 - 1323
