cesium fluoride in neat (no solvent)
byproducts: ClF, CsClF4, F2; stainless-steel cylinder loaded with CsNO3 and CsF, ClF5 (excess) added at -196°C, cylinder agitated on a shaker at 25°C for 18d, cooled back to -196°C; fractional condensation;
参考文献
Christe, Karl O.; Wilson, William W.; Wilson, Richard D.
Inorganic Chemistry, 1989 , vol. 28, p. 675 - 677