1,4-双(苯乙炔基)苯合成路线 （共 41 条）
反应条件
1: lithium phenylacetylide With indium(III) chloride in tetrahydrofuran 2: 1,4-Diiodobenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating;
参考文献
Lee, Phil Ho; Lee, Sung Wook; Seomoon, Dong
Organic Letters, 2003 , vol. 5, # 26 p. 4963 - 4966
反应条件
bis-triphenylphosphine-palladium(II) chloride; oxygen in 1,4-dioxane T=80°C; Sonogashira type coupling;
参考文献
Wang, Xuan; Qin, Weiwei; Kakusawa, Naoki; Yasuike, Shuji; Kurita, Jyoji
Tetrahedron Letters, 2009 , vol. 50, # 46 p. 6293 - 6297
反应条件
[Pd(PPh3)2(OAc)2] in tetrahydrofuran T=66°C; 2 h;
参考文献
Sanechika; Yamamoto; Yammoto
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 752 - 755
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride in toluene T=80°C; Sonogashira coupling; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 66, # 5 p. 1910 - 1913
反应条件
1: potassium hydroxide / H2O; methanol; CHCl3 / 0.5 h / 20 °C 2: 98 percent / CuI; triethylamine / Pd(Ph3P)2Cl2 / 2 h / Heating View Scheme
参考文献
Organic Letters, , vol. 8, # 4 p. 717 - 720
反应条件
SPhos; C16H16Cl2N2O4Pd2; N-hexadecyl-N,N,N-trimethylammonium bromide; triethylamine in water T=130°C; Sonogashira Cross-Coupling; 0.5 h; Microwave irradiation;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 1 p. 203 - 208
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 2 h; Heating;
参考文献
Pena, Miguel A.; Perez Sestelo, Jose; Sarandeses, Luis A.
Synthesis, 2005 , # 3 art. no. Z14204SS, p. 485 - 492
反应条件
1: CuI; triethylamine / Pd(Ph3P)2Cl2 / tetrahydrofuran / 1 h / 20 °C 2: potassium hydroxide / H2O; methanol; CHCl3 / 0.5 h / 20 °C 3: 98 percent / CuI; triethylamine / Pd(Ph3P)2Cl2 / 2 h / Heating View Scheme
参考文献
Organic Letters, , vol. 8, # 4 p. 717 - 720
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 2 h; Heating;
参考文献
Pena, Miguel A.; Perez Sestelo, Jose; Sarandeses, Luis A.
Synthesis, 2005 , # 3 art. no. Z14204SS, p. 485 - 492
反应条件
palladium diacetate; dimethyl sulfoxide T=20°C; Sonogashira Cross-Coupling; 0.0833333 h;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 598 - 605
