1,4-双(苯乙炔基)苯合成路线 （共 41 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in tetrahydrofuran T=40°C; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 24 p. 8922 - 8925
反应条件
piperidine; silica-supported palladium catalyst T=70°C; Sonogashira coupling; 0.5 h;
参考文献
Synthesis, , # 5 p. 829 - 835
反应条件
bis-triphenylphosphine-palladium(II) chloride 16 h; Heating;
参考文献
Gelman, Dmitri; Tsvelikhovsky, Dmitry; Molander, Gary A.; Blum, Jochanan
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6287 - 6290
反应条件
T=500°C; Elimination; P=0.01 Torr; 2 h;
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Hill, Lawrence; Lumbard, Keith W.; Maccallum, James R.; Seth, Shirley
Tetrahedron, 1999 , vol. 55, # 36 p. 11039 - 11050
反应条件
bis(acetylacetonato) palladium; triphenylphosphine in tetrahydrofuran T=40°C; 4 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 35, # 2 p. 397 - 401
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 2 p. 429 - 433
反应条件
1: (i) NaNH2, liq. NH3, Et2O, (ii) /BRN= 773967/ 2: SnCl2, aq. HCl / tetrahydrofuran View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 34, p. 1827 - 1832
反应条件
1: 94 percent / dimethylformamide / Heating 2: 36 percent / BuLi / tetrahydrofuran; hexane / 12 h 3: 44 percent / 2 h / 500 °C / 0.01 Torr View Scheme
参考文献
Tetrahedron, , vol. 55, # 36 p. 11039 - 11050
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 2043 - 2045
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2213 - 2215
反应条件
potassium hydroxide; butan-1-ol
参考文献
Chemische Berichte, , vol. 91, p. 1274,1277
反应条件
potassium tert-butylate; bromine 1) CHCl3, 1 h, 2) THF, 30 min, reflux; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 755 - 758
