1.1: NaH / tetrahydrofuran / 0.67 h / 0 - 20 °C 1.2: 96 percent / tetrahydrofuran / 3 h / 20 °C 2.1: 89 percent / NaOH; water / ethanol / 1 h / 20 °C View Scheme
参考文献
Baker,B.R.; Ashton,W.T.
Journal of Medicinal Chemistry, 1970 , vol. 13, p. 1165 - 1170
1: 68 percent / C5H11ONa / pentan-1-ol / 8 h / 130 °C 2: 80 percent / H2 / Raney nickel / bis-(2-methoxy-ethyl) ether / 0.5 h / 100 °C / 76000 Torr View Scheme
参考文献
Gordeev, E. N.; Buyanov, V. N.; Zhigachev, V. E.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 1 p. 40 - 42
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 1 p. 46 - 48
