3-溴-5-氯-4-羟基苯甲醛合成路线 （共 4 条）
反应条件
bromine in acetic acid T=80°C; 24 h;
参考文献
Speicher, Andreas; Kolz, Juergen; Sambanje, Rufino Paulino
Synthesis, 2002 , # 17 p. 2503 - 2512
反应条件
1.1: NCS / CHCl3 / 1 h / 60 °C 1.2: 76 percent / aq. HCl / CHCl3 / 12 h / 60 °C 2.1: 60 percent / Br2 / acetic acid / 24 h / 80 °C View Scheme
参考文献
Cossey,H.D. et al.
Journal of the Chemical Society, 1965 , p. 954 - 973
反应条件
perchloric acid electrolysis at 0.13 mA/cm2, 1.4 F/mol, C.C.E. 919 --> 1101 mV vs SCE; electrolyte LiClO4; Product distributionMechanism;
参考文献
Takahashi, Masakatsu; Konishi, Hironori; Iida, Satoshi; Nakamura, Kensuke; Yamamura, Shosuke; Nishiyama, Shigeru
Tetrahedron, 1999 , vol. 55, # 17 p. 5295 - 5302
反应条件
sodium hydroxide T=100°C; 0.166667 h;
参考文献
Speicher, Andreas; Kolz, Juergen; Sambanje, Rufino Paulino
Synthesis, 2002 , # 17 p. 2503 - 2512
