(3Z)-7,7-二乙氧基-3-庚烯合成路线 （共 7 条）
反应条件
iso-propylmagnesium bromide; NiCl2((PPh3)P)2 in tetrahydrofuran; diethyl ether Heating;
参考文献
Trost, Barry M.; Ornstein, Paul L.
Tetrahedron Letters, 1981 , vol. 22, # 36 p. 3463 - 3466
反应条件
1: 1.) KOt-C4H9, 2.) C5H5N / 1.) THF, 0 deg C - -78 deg C - RT, 2.) (C2H5)2O, RT 2: 454 - 650 °C / 0.05 - 0.3 Torr / flash vacuum pyrolysis 3: HCl / ethanol 4: 65 percent / 2-propylmagnesium bromide / (Ph3P)2NiCl2 / tetrahydrofuran; diethyl ether / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 22, # 36 p. 3463 - 3466
反应条件
1: HCl / ethanol 2: 65 percent / 2-propylmagnesium bromide / (Ph3P)2NiCl2 / tetrahydrofuran; diethyl ether / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 22, # 36 p. 3463 - 3466
反应条件
1: 454 - 650 °C / 0.05 - 0.3 Torr / flash vacuum pyrolysis 2: HCl / ethanol 3: 65 percent / 2-propylmagnesium bromide / (Ph3P)2NiCl2 / tetrahydrofuran; diethyl ether / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 22, # 36 p. 3463 - 3466
反应条件
1: PBr3, Py 2: (i) Mg, (ii) /BRN= 1719716/ View Scheme
参考文献
Synthesis, , p. 379 - 380
反应条件
(i) Mg, (ii) /BRN= 1719716/; Multistep reaction;
参考文献
Synthesis, , p. 379 - 380
参考文献
Stetter,H.; Kuhlmann,H.
Synthesis, 1975 , p. 379 - 380
